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85results about How to "Efficient precipitation" patented technology

Technology for recycling platinum and palladium from acid solution containing low concentration of platinum family precious metals by adopting reducing precipitation method

InactiveCN103421956AEfficient precipitationLow supernatant platinum and palladium contentProcess efficiency improvementPlatinumRefining (metallurgy)
The invention discloses a method for recycling platinum and palladium from precious metal acid solution by adopting a reducing precipitation method, and belongs to the technical field of metallurgy. The method comprises the following steps: enabling a reducing precipitation agent formed by sodium formate and sodium borohydride to react with material liquid containing platinum and palladium, so as to precipitate platinum and palladium; filtering precipitation; dissolving base metals in the precipitation by dilute sulphuric acid; further, dissolving precipitation residues containing platinum and palladium by dilute sulphuric acid and sodium chlorate; finally, obtaining chlorination liquid containing a great amount of platinum and palladium, concentrating the chlorination liquid, and refining to recycle platinum and palladium through performing the process of precipitating platinum by ammonium chloride on the chlorination liquid. According to the invention, the technology is simple and low in cost, and generates little pollution; the precipitation rate of platinum and palladium precious metals can reach over 99.9%, the platinum family metal recycling ratio is greatly improved, and the comprehensive utilization of precious metal resources is realized.
Owner:NORTHWEST NORMAL UNIVERSITY

Stirring cooking device for traditional Chinese medicinal materials

The invention discloses a stirring type Chinese herbal medicine cooking equipment, which comprises a support seat, a support frame is connected to both sides of the upper end of the support seat, a first rack is connected to the upper end of the support frame, a first gear is meshed in the middle part of the front end of the first rack, and a first gear is engaged with the first rack. The middle part of the lower end of the first gear is connected with the stirring shaft, the right side of the upper end of the support base is connected with the driving box, the second gear is arranged inside the driving box, the lower end of the second gear is meshed with the second rack, and the left end of the second rack is connected with the right swing rod. The cooking barrel is connected to the left side of the right swing lever, the left swing lever is connected to the lower side of the left end of the cooking barrel, and the middle part of the left end of the left swing lever is covered with a return spring, and the left end of the return spring is connected to a rotating block. There is a heating ring inside the cooking barrel. The upper end of the side is connected with a hopper, and the middle part of the bottom end of the cooking barrel is connected with a discharge hopper. The present invention realizes the rotation of the stirring shaft, so that the active ingredients inside the traditional Chinese medicine can be effectively separated out, and at the same time realizes the left and right reciprocating shaking of the cooking barrel.
Owner:陈忠民

Medium and low coal temperature separate dry distillation system and method

The invention provides a medium and low coal temperature separate dry distillation system and method. The dry distillation system comprises a spiral pushing medium and low temperature external heating dry distillation device and a low temperature internal heating rotary kiln dry distillation device. A spiral pushing dry distillation chamber in the spiral pushing medium and low temperature external heating dry distillation device is arranged in a combustion chamber of the spiral pushing medium and low temperature external heating dry distillation device, burned smoke in the combustion chamber is circulated back into a rotary kiln cylinder, and solid-state materials in the rotary kiln cylinder are supplied into the spiral pushing dry distillation chamber. For the first time, dry distillation of coal is divided into two or more stages according to temperature, an internal heating rotary kiln and the external heating type spiral pushing dry distillation device are combined organically to achieve dry distillation; the rotary kiln is used for performing winnowing dust removal, preheating drying and dehydration on raw coal, and the external heating type spiral pushing dry distillation device realizes a high-efficiency medium and low temperature dry distillation process and precipitation of high calorific value raw gas and a tar product; the advantages of internal and external heating dry distillation equipment are fully combined, dry distillation efficiency, heat utilization efficiency and dry distillation product quality are greatly improved in a brand new mode, and the market popularization prospect is broad.
Owner:王崇峰

Purifying, condensing and storing tank for gas

The invention provides a purifying, condensing and storing tank for gas. The tank comprises outer arrangement and inner arrangement. The outer arrangement and the inner arrangement are composed of an inlet valve, a slag removal valve, a drain valve, a coagulant valve, a pure gas valve, a bent filter tube, a separation tank, a purification tank, a coagulant tank, a gas storage tank, and a purification tube, wherein the inlet valve is arranged at one side of the upper end of the gas storage tank, the slag removal valve is arranged at one side of the lower end of the gas storage tank, the drain valve is installed at one side of the lower end of the gas storage tank, the coagulant valve is mounted at one side of the lower end of the gas storage tank, the pure gas valve is arranged at an upper side of the gas storage tank, the bent filter tube is mounted at the inner side of the upper end of the gas storage tank and comprises two sets of identical bent pipes, the separation tank is arranged at the inner side of the gas storage tank, the central part of the separation tank is provided with a microfiltration mesh, the purification tank is arranged at one side of the separation tank, a back-pressure valve at the lower side of the purification tank is communicated with the separation tank, the coagulant tank is arranged at the lower side in the gas storage tank and is communicated with the coagulant valve, the gas storage tank is arranged at the outer sides of the separation tank and the coagulant tank, and the purification tube is arranged at one side of the separation tank and is communicated with the bent filter tube. The purifying, condensing and storing tank for gas provided by the invention has the advantages of an exquisite design structure, advanced technical characteristics, multiple functions, practicality, convenience, slag removal and purification of draining, high-quality purification, condensation and storage of gas, high efficiency, energy saving and environmental protection.
Owner:LIUZHOU JINGYANG ENERGY SAVING TECH RES DEV

Mechanical method and apparatus for removing polycarprolactam dimers

The invention discloses a mechanical method for removing polycarprolactam cyclic oligomer. The method comprises the following steps: (1) cooling caprolactam concentrate which has undergone triple effect evaporative concentration and has a temperature of 110 to 130 DEG C for crystallization, and carrying out stirring with a stirrer when the temperature of the caprolactam concentrate drops to 50 to 95 DEG C; (2) prefiltering the cooled concentrate, carrying out pressurization with a pressurization device until the concentrate has a pressure of 0.4 to 0.6 MPa, and allowing the concentrate to enter into aplate and frame type filter press for press filtration so as to obtain clear liquid of the caprolactam concentrate; (3) storing the clear liquid in a clear liquid storage tank, adding the clear liquid of the caprolactam concentrate into a fresh caprolactam storage tank through a metering pump, mixing the clear liquid with fresh caprolactam, and allowing an obtained mixture to enter into a polymerization reactor. The method provided in the invention enables flow for removing polycarprolactam cyclic oligomer to be simplified and a high removal rate of annular oligomers in the caprolactam concentrate to be obtained; the apparatus in the invention has the advantages of a large filtering area, a strong capability of bearing pollutants, convenience in cleaning and low cost.
Owner:浙江华建尼龙有限公司

Internal and external heating type medium and low temperature powdered coal temperature division dry distillation system and method

The invention discloses an internal and external heating type medium and low temperature powdered coal temperature division dry distillation system and method. The system comprises a spiral pushing medium and low temperature external heating dry distillation device and a low temperature internal heating rotary kiln dry distillation device, wherein a spiral pushing dry distillation chamber in the spiral pushing medium and low temperature external heating dry distillation device is arranged in a combustion chamber of the spiral pushing medium and low temperature external heating dry distillation device, combustion smoke in the combustion chamber is directly supplied to the interior of a rotary kiln cylinder, and solid materials in the rotary kiln cylinder are supplied to the interior of the spiral pushing dry distillation chamber. Dry distillation of coal is divided into two or more phases according to temperature and is achieved through organic combination of the internal heating rotary kiln dry distillation device and the spiral pushing external heating dry distillation device, winnowing and dust removal, preheating and drying and dehydration are conducted on raw coal by means of a rotary kiln, high-efficiency medium and low temperature dry distillation and high-calorific-value raw gas and tar product precipitation are achieved by means of the spiral pushing external heating dry distillation device, the advantages of the internal heating dry distillation device and the external heating dry distillation are fully combined, dry distillation efficiency, heat utilization efficiency and the quality of dry distillation products are improved greatly, and marketing prospects are broad.
Owner:王崇峰
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