Polymer of fatty alcohol polyethenoxy ether class, and application as economization agent for concrete
A technology of alcohol polyoxyethylene ether and concrete shrinkage reducing agent, which is applied in the field of concrete shrinkage reducing agent, can solve the problems of difficulty in wide application, toxicity, and high cost of shrinkage reducing agent, and achieve the effects of being beneficial to environmental protection, simple production process, and low production cost
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Embodiment 1
[0026] This embodiment is the preparation of shrinkage reducing agent, raw material has: C 12 ~C 18 Fatty alcohol; Ethylene oxide; Acetic acid; Hydrogen peroxide; Sodium hydroxide. The preparation process is: combine ethylene oxide with C 12 ~C 18 Fatty alcohol is mixed in a ratio of 5:1 by weight, and then sodium hydroxide is added as a catalyst. The amount of sodium hydroxide added is 0.15% of the weight of ethylene oxide, and the condensation reaction is carried out at normal pressure and 170°C to 180°C. The time is about 2 hours. After the reaction is completed, neutralize with acetic acid to pH 7, and bleach with hydrogen peroxide at 70°C to obtain the concrete shrinkage reducer of the present invention.
Embodiment 2
[0028] This example is a concrete test.
[0029] 1. Concrete raw materials for testing
[0030] Cement——42.5R and 52.5R ordinary Portland cement; silica fume; high-efficiency water reducing agent, water reducing rate above 25%; limestone crushed stone coarse aggregate, river sand, fineness modulus 2.4; expansion agent; shrinkage reducing agent (prepared by the method of Example 1).
[0031] 2. Test concrete mix ratio
[0032] The water-binder ratio of concrete used in the test is 0.18, the amount of water reducing agent is 2.5% of the weight of the cementing material, and the amount of shrinkage reducing agent is 0.5% to 1.0% of the weight of the cementing material. A total of 8 groups of concrete samples are formed. The specific combination Such as shown in Table 1. .The shrinkage reducing agent is mixed with other concrete components in the form of solid powder.
[0033] concrete
sample
water-binder ratio
Binder
Dosag...
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