The invention relates to the field of
fiber membrane preparation, in particular to a preparation and test method of a
microfiltration composite
fiber membrane, which comprises the following steps: preparing a PVA (
Polyvinyl Alcohol) solution; accurately and respectively weighing CA and GO, and respectively adding the CA and the GO into the prepared PVA solution to obtain a PVA / CA / GO
spinning solution; assembling SVF base cloth on an unwinding mechanism,
coating the front end of the base cloth on the surface of a
metal mesh curtain above a solution tank, then pouring a
spinning solution into the solution tank, and performing electrostatic
spinning after adjusting spinning conditions to obtain a composite
fiber membrane; the composite fiber membrane is subjected to
hot pressing treatment, so that carboxyl on a cross-linking agent
citric acid and hydroxyl of a PVA chain are subjected to an
esterification reaction,
water resistance is improved through structural regulation and control of a PVA
polymer, and the
microfiltration composite fiber membrane is obtained. According to the invention, the contact area of the cross-linking agent
citric acid and PVA is greatly increased, so that the cross-linking effect is more sufficient, and the fiber membrane can maintain a good fiber form after working in water for a long time.