Method for synthesizing isotropic silicon nitride powder adopting hollow type annular material-distribution
A technology for combustion synthesis and silicon nitride powder, which is applied in chemical instruments and methods, nitrogen compounds, inorganic chemistry, etc. Powder production efficiency and product purity, synthetic product composition and uneven microscopic morphology, etc., to avoid heat accumulation, high α-phase content, and uniform and fine particles
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Embodiment 1
[0046] The raw materials used in this example are silicon powder with an average particle size of 25 μm (purity greater than 98.5%) and silicon nitride powder with an average particle size of 1 μm (purity greater than 96%, and α-phase content of about 93%). Dosing and grinding and mixing according to the weight ratio, the proportioning ratio is Si:Si 3 N 4 =50:50, the total weight of the reaction mixture was 4.2 kg. The above-mentioned grinding and mixing of the reaction mixture is carried out in the following manner: first, the silicon powder is ground and mixed in the ball mill barrel of the agitating ball mill with absolute ethanol as the ball milling medium for 6 hours, and then dried in a vacuum oven at 60°C. Then add inert diluent silicon nitride powder and grind and mix on a vibrating mill for 1 hour. The reaction mixture was then placed in a cylindrical porous graphite crucible according to the attached figure 1 The hollow annular cloth is shown, wherein the cylindr...
Embodiment 2
[0049] The raw materials used in this example are silicon powder with an average particle size of 17 μm (purity greater than 98%) and silicon nitride powder with an average particle size of 2.2 μm (purity greater than 98%, and α-phase content of about 95%). Dosing and grinding and mixing according to the weight ratio, the proportioning ratio is Si:Si 3 N 4=52.5:47.5, the total weight of the reaction mixture was 4 kg. The above-mentioned grinding and mixing of the reaction mixture is carried out in the following manner: first mix the silicon powder and the inert diluent silicon nitride powder in the ball mill barrel of the agitating ball mill with absolute ethanol as the ball milling medium for ball milling for 8 hours for grinding and mixing, and then grind and mix in the electric heating Drying was performed in an oven at 65°C. Then the dried silicon powder and the inert diluent silicon nitride powder mixture were ground and mixed on a roller mill for 2 hours. Then the rea...
Embodiment 3
[0051] The raw materials used in this example are silicon powder with an average particle size of 47 μm (purity greater than 98.5%) and silicon nitride powder with an average particle size of 1.5 μm (purity greater than 96%, and α-phase content of about 90%). Dosing and grinding and mixing according to the weight ratio, the proportioning ratio is Si:Si 3 N 4 =55:45, the total weight of the reaction mixture was 3.5 kg. The above-mentioned grinding and mixing of the reaction mixture is carried out in the following manner: first, the silicon powder and the inert diluent silicon nitride powder are respectively ball milled in the ball mill barrel of the agitating ball mill with absolute ethanol as the ball mill medium for 6 hours, and then in a vacuum oven at 60 °C for drying. The mixture of silicon powder and silicon nitride powder, an inert diluent, was then ground and mixed on a vibrating mill for 3 hours. Then these three reaction mixtures with different component ratios wer...
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