Bitumen compositions and preparation method thereof
A technology of asphalt composition and polymer, which is applied in the direction of building structure, building components, building insulation materials, etc., and can solve the problems of insufficient research on modified emulsified asphalt
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Embodiment 1
[0042] (1) Preparation of modified asphalt: heating No. 90 petroleum asphalt with 89.1% mass percentage to 175~185°C to a fluid state, adding 7% reverse sequence furfural to extract oil and 3.8% polymer ( The polymer comprises 40% star-shaped SBS and 60% linear SBS), then through the colloid mill grinding at 2500RPM, then swelled under stirring for 4 hours, then added 0.1% sulfur powder, and reacted for 3 hours to prepare Dede modified asphalt;
[0043] (2) Soap liquid preparation: be 0.9% emulsifying agent (emulsifying agent comprises 30% cetyl dimethyl hydroxyethyl ammonium chloride, 30% 1-aminoethyl-2-tetradecyl ~ octadecyl imidazoline, 30% nonylphenol ethoxylate NP-7, 5% isopropanol and 5% water), 0.15% calcium chloride, 0.03% hydroxypropyl methylcellulose Add plain and 0.03% sepiolite to water at a temperature of 40-60°C, add the water to 100%, adjust the pH value of the soap solution to 1.5-2.5 with concentrated hydrochloric acid, and stir evenly to obtain a soap soluti...
Embodiment 2
[0046] (1) Modified asphalt preparation: the No. 110 petroleum asphalt that is 87.06% by mass is heated to 175~185 ℃ to flow state, add 8.5% reverse sequence furfural to extract oil successively, 4.3% polymer ( The polymer comprises 35% star-shaped SBS and 65% linear SBS), then through the colloid mill grinding of 3000RPM, then swelled under stirring for 5 hours, then added 0.06% organic polysulfide and 0.08% Sulfur powder was reacted for 3.5 hours to obtain modified asphalt;
[0047] (2) Soap liquid preparation: be 1% emulsifier (the emulsifier comprises 35% cetyl dimethyl hydroxyethyl ammonium chloride, 30% octadecyl propylene diamine, 25% emulsifier) % of octylphenol ethoxylate OP-10, 5% of acetone and 5% of water), 0.18% of ammonium chloride, 0.03% of sodium carboxymethylcellulose and 0.02% of meerschaum were added to the temperature In water at 40-60°C, add the water to 100%, adjust the pH of the soap solution to 1.5-2.5 with concentrated hydrochloric acid, stir evenly, ...
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