Method for synthesizing adsorption functional material for number one Sudan red
A technology of functional materials and synthesis methods, applied in chemical instruments and methods, and other chemical processes, can solve the problems of slow mass transfer and difficult elution, and achieve easy elution, fast mass transfer, and easy control of reaction conditions Effect
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[0015] Below in conjunction with embodiment, the present invention is further described; Following embodiment is illustrative, not limiting, can not limit protection scope of the present invention with following embodiment.
[0016] The invention combines the surface molecular imprinting technology and the sol-gel technology to imprint the amine functional group on the surface of the silicon ball, thereby synthesizing the functional material with high selective adsorption for Sudan Red I. Its specific embodiment is:
[0017] 1. Add 14mL of acetonitrile, 0.5g of Sudan Red I, 1.8mL of 3-aminopropyltriethoxysilane containing bifunctional groups and 0.4g of silicon spheres activated by methanesulfonic acid aqueous solution into a 100ml three-path bottle in sequence , Stir the reaction under reflux for 35 minutes, then add 1.8mL tetraethoxysilane and 1.2mL 0.1mol L -1 acetic acid, incubate at 60°C for 9 hours.
[0018] 2. Filter the above product through ethanol and age it at 100...
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