Method for preparing earthwork synthetic material adhesive
A technology of geosynthetic materials and adhesives, applied in the direction of adhesive types, amide/imide polymer adhesives, etc., can solve the problem of reducing the permeability of bentonite, affecting the anti-seepage performance of materials, and poor hydrolysis resistance, etc. problems, to achieve low cost, overcome easy cracking, and fast gelation
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[0020] 1. Synthesis process of modified polyacrylamide
[0021] Weigh 8-11 grams of acrylamide, 85-96 grams of water, ammonium persulfate (initiator, the concentration is 3.0×10 -3 mol / L), sodium formate (chain transfer agent, the concentration is 8×10 -2 mol / L). First, add the weighed sodium formate and part of water into the reactor equipped with stirrer, condenser and thermometer, turn on the heater and stirrer at the same time, pour part of the acrylamide solution into the four-necked bottle, and put the remaining solution into Dropping funnel.
[0022] When the temperature reaches above 60°C, add the prepared ammonium persulfate, and when the temperature reaches 80°C, start to add the remaining acrylamide solution dropwise, and react for 2 hours after the dropwise addition.
[0023] Continue to adjust the temperature to 40°C and the pH value (using triethylamine) to 10, add formaldehyde at constant temperature and control the pH value at any time, and stop heating afte...
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