A kind of high temperature resistant flexible one-component epoxy sealing adhesive and preparation method thereof
A technology of epoxy sealing and high temperature flexibility, applied in epoxy resin glue, adhesives, adhesive additives, etc., can solve the problems of low bonding strength and low yield of silicone
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Embodiment 1
[0072] A high-temperature-resistant flexible one-component epoxy sealing adhesive prepared from the following raw materials in parts by weight:
[0073] Epoxy resin: 20 parts of bisphenol F epoxy resin YLE1300F;
[0074] Softening resin: HEF750 26 parts;
[0075] Softening resin: 4 parts of H2004;
[0076] Reactive diluent: 20 parts of tertiary carbonic acid glycidyl ether E10P;
[0077] Curing agent: 2.6 parts of modified imidazole latent thermal curing agent PN-23;
[0078] Curing agent: modified amine latent thermal curing agent EH-4360S 7 parts;
[0079] Inhibitor: 0.1 part of 2,6-di-tert-butyl-p-cresol BHT;
[0080] Fumed silica: 5 parts of R8200;
[0081] Wetting flow promoter: MEGAFACE F-560 0.3 parts;
[0082] Spherical silica powder: 15 parts of Q010.
[0083] The preparation method of adhesive in the present embodiment comprises the following steps:
[0084] 1) Add epoxy resin, mixed softening resin, fumed silica, and spherical silicon micropowder into the st...
Embodiment 2
[0089] A high-temperature-resistant flexible one-component epoxy sealing adhesive prepared from the following raw materials in parts by weight:
[0090] Epoxy resin: 20 parts of bisphenol F epoxy resin YLE1300F;
[0091] Softening resin: 22 parts of HEF750;
[0092] Softening resin: 8 parts of H2004;
[0093] Reactive diluent: 20 parts of tertiary carbonic acid glycidyl ether E10P;
[0094] Curing agent: 2.6 parts of modified imidazole latent thermal curing agent PN-23;
[0095] Curing agent: modified amine latent thermal curing agent EH-4360S 7 parts;
[0096] Inhibitor: 0.1 part of 2,6-di-tert-butyl-p-cresol BHT;
[0097] Fumed silica: 5 parts of R8200;
[0098] Wetting flow promoter: MEGAFACE F-560 0.3 parts;
[0099] Spherical silica powder: 15 parts of Q010.
[0100] The preparation method of the adhesive in this example is consistent with Example 1.
Embodiment 3
[0102] A high-temperature-resistant flexible one-component epoxy sealing adhesive prepared from the following raw materials in parts by weight:
[0103] Epoxy resin: 20 parts of bisphenol F epoxy resin YLE1300F;
[0104] Softening resin: HEF750 18 parts;
[0105] Softening resin: 12 parts of H2004;
[0106] Reactive diluent: 20 parts of tertiary carbonic acid glycidyl ether E10P;
[0107] Curing agent: 2.6 parts of modified imidazole latent thermal curing agent PN-23;
[0108] Curing agent: modified amine latent thermal curing agent EH-4360S 7 parts;
[0109] Inhibitor: 0.1 part of 2,6-di-tert-butyl-p-cresol BHT;
[0110] Fumed silica: 5 parts of R8200;
[0111] Wetting flow promoter: MEGAFACE F-560 0.3 parts;
[0112] Spherical silica powder: 15 parts of Q010.
[0113] The preparation method of the adhesive in this example is consistent with Example 1.
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