Process technique for extracting tea polyphenol from tree plant flower
A processing technology and technology of tea tree flowers, which are applied in the preparation of organic compounds, chemical instruments and methods, organic chemistry, etc., can solve the problems of low purity of tea polyphenols, single separated components, and difficulty in expanding the scale. The effect of richness, high physical and chemical stability, and high operating cost
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Embodiment 1
[0021] Fresh tea tree flowers harvested on site are dried in low-temperature vacuum to obtain dry tea tree flowers, which reduces the oxidation loss of polyphenols during preservation. The tea tree flower grinder is crushed to about 50 meshes, 3kg of crushed tea tree flowers are mixed with 60 L of 60% ethanol, after cold soaking for 8 hours, put into a temperature-controlled ultrasonic extraction equipment, heated to 55°C, ultrasonically extracted for 20 minutes, and filtered; the second time Add 30 L of 60% ethanol for extraction, heat to 55°C, ultrasonically extract for 5 minutes, and filter. The two filtrates were combined. The filtrate is concentrated in vacuum to recover ethanol, the volume fraction of ethanol in the extract is reduced, and water is added to make up to 100L. Microfiltration clarifies the tea tree flower extract, removes a large amount of tea tree flower fine particles and suspended impurities in the material liquid, and reduces the pollution to the subse...
Embodiment 2
[0027] Fresh tea tree flowers harvested on site are dried in low-temperature vacuum to obtain dry tea tree flowers, which reduces the oxidation loss of polyphenols during preservation. The tea tree flower grinder is crushed to about 50 meshes, 3 kg of crushed tea tree flowers are mixed with 70 L of 60% ethanol, after cold soaking for 4 hours, put into a temperature-controlled ultrasonic extraction equipment, heated to 60 ° C, ultrasonically extracted for 30 minutes, and filtered; the second For the second extraction, add 30 L of 60% ethanol, heat to 60°C, ultrasonically extract for 5 minutes, and filter. The two filtrates were combined. The filtrate is concentrated in vacuum to recover ethanol, the volume fraction of ethanol in the extract is reduced, and water is added to make up to 100L. Microfiltration clarifies the tea tree flower extract, removes a large amount of tea tree flower fine particles and suspended impurities in the material liquid, and reduces the pollution to...
Embodiment 3
[0033] Fresh tea tree flowers harvested on site are dried in low-temperature vacuum to obtain dry tea tree flowers, which reduces the oxidation loss of polyphenols during preservation. The tea tree flower grinder is crushed to about 50 meshes, 3kg of crushed tea tree flowers are mixed with 75L of 60% ethanol, after cold soaking for 9 hours, put into a temperature-controlled ultrasonic extraction equipment, heated to 50°C, ultrasonically extracted for 25 minutes, and filtered; the second extraction Add 30 L of 60% ethanol, heat to 50°C, ultrasonically extract for 5min, and filter. The two filtrates were combined. The filtrate is concentrated in vacuum to recover ethanol, the volume fraction of ethanol in the extract is reduced, and water is added to make up to 100L. Microfiltration clarifies the tea tree flower extract, removes a large amount of tea tree flower fine particles and suspended impurities in the material liquid, and reduces the pollution to the subsequent ultrafilt...
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