Magnetorheologicai polishing liquid and preparation method thereof
A technology of magnetorheological polishing and polishing powder, which is applied in the directions of magnetic liquids, polishing compositions, chemical instruments and methods, etc., can solve the problems of undiscovered reports or literature, unsuitable for magnetorheological polishing, unsuitable for optical polishing, etc. Achieve good anti-settling and agglomeration stability, good polishing effect and consistent performance
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Embodiment 1
[0038] Embodiment 1: magnetorheological polishing liquid is made up of magnetic particles, purified water, additive, surfactant and polishing powder, and its volume percentage is:
[0039] Magnetic particles 30%
[0040] Purified water 50%
[0041] Additive 7%
[0042] Surfactant 5%
[0043] Polishing powder 8%
[0044] The additive is a stabilizer, and the magnetic particles are suspended phases of iron powder with an average particle size of ≤3.5um.
[0045] The preparation method is to firstly carry out surface purification and activation treatment on the magnetic particles. In this example, the magnetic particles are carbonyl iron powder particles. The specific preparation process is carried out according to the following steps:
[0046] 1. Weigh the magnetic particles by volume percentage and put them into the ball mill jar;
[0047]2. Take the surfactant by volume percentage and mix it with ethanol equivalent to 50% of the volume of the magnetic particles, and shake...
Embodiment 2
[0059] Embodiment 2: manufacture step is with embodiment 1, and concrete selected composition is mostly also with embodiment 1, but the volume percent of each composition is respectively:
[0060] Magnetic particles 35%
[0061] Purified water 50%
[0062] Additive 5%
[0063] Surfactant 5%
[0064] Polishing powder 5%
[0065] In this embodiment, organic bentonite is selected as the additive; in the third step of the preparation process, the rotational speed of the ball mill is 200 rpm when the surfactant is mixed with the magnetic particles. The zero-field viscosity of the magnetorheological fluid at room temperature is 800mPa.s, without obvious sedimentation and compaction, and can be suspended again under the action of a weak magnetic field.
[0066] The magnetorheological polishing liquid is used to polish K9 glass on the magnetorheological polishing machine of Xi'an Technological University. After 30 minutes, the roughness Sa of the processed surface can reach 1.8nm,...
Embodiment 3
[0067] Embodiment 3: carry out embodiment 1 repeatedly by described same step, but the volume percent of each composition is:
[0068] Magnetic particles 40%
[0069] Purified water 45%
[0070] Additive 5%
[0071] Surfactant 5%
[0072] Polishing powder 5%
[0073] In this embodiment, except that polyethylene glycol is selected as the surfactant, the other specific selected ingredients are the same as in Example 1. In the third step of the preparation process, the ball milling speed is 500 rpm when mixing the surfactant and the magnetic particles. The zero-field viscosity of the magnetorheological fluid at room temperature is 1050mPa.s, without obvious sedimentation and compaction, and can be suspended again under the action of a weak magnetic field.
[0074] The magnetorheological polishing liquid is used to polish the K9 glass plane on the magnetorheological polishing machine of Xi'an University of Technology. After 30 minutes, the roughness Sa of the processed surface...
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