Ba1-xMgLiGaMxFBr1-ySy:Rez'Ag0.1 optical storage luminescent material and preparation method thereof
A technology for luminescent materials and optical storage, applied in luminescent materials, chemical instruments and methods, etc., can solve problems such as blurred images, unreadable images, and bulky volume, so as to improve the convenience of use, increase the elastic range, and improve the luminous performance Effect
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Embodiment 1
[0032] with Ba 0.9 MgLiGaSi 0.1 FBr 0.9 S 0.1 :Eu 0.08 , Ag 0.1 As an example, according to the stoichiometric ratio, the BaCO 3 , MgCO 3 , LiCO 3 , Ga 2 o 3 , AgNO 3 , NH 4 F, NH 4 Br, sulfur powder, SiO 2 , Eu2 o 3 Mix and add ethanol to fully grind, then heat the raw material at 60°C for drying; use solid-state reaction, surround the ground raw material with activated carbon powder and burn for 3 hours in a reducing atmosphere at a high temperature of 800°C. Cool to room temperature; grind the sample and sieve it, wash it twice with ethanol, heat the sample at 60°C to dry; mix the dried sample with methyl methacrylate solution of 1 / 2 the mass of the sample, and dry at 120°C for 2 After hours, grind the sample and sieve it, wash it twice with ethanol, heat the sample at 60°C for drying, and then screen-coat it.
Embodiment 2
[0034] with Ba 0.7 MgLiGaTi 0.3 FBr 0.6 S 0.4 : Dy 0.06 , Ag 0.1 As an example, according to the stoichiometric ratio, the BaCO 3 , MgCO 3 , LiCO 3 , Ga 2 o 3 , AgNO 3 , NH 4 F, NH 4 Br, sulfur powder, TiO 2 , Dy 2 o 3 Mix and add ethanol to fully grind, then heat the raw material at 50°C for drying; use solid-state reaction, surround the ground raw material with activated carbon powder and burn for 3 hours in a reducing atmosphere at a high temperature of 900°C. Cool to room temperature; grind the sample and sieve it, wash it twice with ethanol, heat the sample at 50°C for drying; mix the dried sample with methyl methacrylate solution of 1 / 2 the mass of the sample, and dry at 120°C for 2 After hours, grind the sample and sieve it, wash it twice with ethanol, heat the sample at 60°C for drying, and then screen-coat it.
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