Oxidation treatment method for carrier carbon surface
An oxidation treatment, carrier carbon technology, applied in chemical instruments and methods, catalyst carriers, chemical/physical processes, etc., can solve the problem of small specific surface area methylene blue adsorption value, low dispersion of precious metal active components, and oxygen-containing functional groups ash. The problem of high content, to achieve the effect of improving performance, short processing time, increasing alkalinity and specific surface area
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specific Embodiment approach 2
[0030] A method for oxidation treatment of a carrier carbon surface, comprising the following steps
[0031] (1) acid treatment
[0032] The powdered activated carbon and the nitric acid solution with a weight concentration of 2-12% are mixed in a ratio of 1:7 by weight, and treated at a temperature of 30-50° C. for 1-2 hours,
[0033] (2) Filtration and washing
[0034] Filter the powdered activated carbon suspension treated in step (1), wash the filter residue with water until the pH value of the washing water is 6.5-7,
[0035] (3) Ultrasonic radiation treatment
[0036] The powdered activated carbon and water prepared in step (2) are formulated into a suspension in a weight ratio of 1:7, and the suspension is subjected to ultrasonic radiation treatment for 20-120min at a temperature of 30-60°C, wherein the ultrasonic Energy control at 1-10W / cm 2 between,
[0037] (4) Microwave treatment
[0038] After the powdered activated carbon obtained by filtering the obtained s...
specific Embodiment approach 3
[0039] A method for oxidation treatment of a carrier carbon surface, comprising the following steps
[0040] (1) acid treatment
[0041] The powdered activated carbon and the nitric acid solution with a weight concentration of 2-12% are mixed in a ratio of 1:10 by weight, and treated at a temperature of 30-50° C. for 1-2 hours,
[0042] (2) Filtration and washing
[0043] Filter the powdered activated carbon suspension treated in step (1), wash the filter residue with water until the pH value of the washing water is 6.5-7,
[0044] (3) Ultrasonic radiation treatment
[0045] The powdered activated carbon and water prepared in step (2) are formulated into a suspension in a weight ratio of 1:4, and the suspension is subjected to ultrasonic radiation treatment for 20-120min at a temperature of 30-60°C, wherein the ultrasonic Energy control at 1-10W / cm 2 between,
[0046] (4) Microwave treatment
[0047] After the powdered activated carbon obtained by filtering the obtained ...
specific Embodiment approach 4
[0048] A method for oxidation treatment of a carrier carbon surface, comprising the following steps
[0049] (1) acid treatment
[0050] Mix powdered activated carbon and nitric acid solution with a weight concentration of 2-12% in a ratio of 1:6 by weight, and treat at a temperature of 30-50°C for 1-2 hours,
[0051] (2) Filtration and washing
[0052] Filter the powdered activated carbon suspension treated in step (1), wash the filter residue with water until the pH value of the washing water is 6.5-7,
[0053] (3) Ultrasonic radiation treatment
[0054] The powdered activated carbon and water prepared in step (2) are formulated into a suspension in a weight ratio of 1:10, and the suspension is subjected to ultrasonic radiation treatment for 20-120min at a temperature of 30-60°C, wherein the ultrasonic Energy control at 1-10W / cm 2 between,
[0055] (4) Microwave treatment
[0056] After the powdered activated carbon obtained by filtering the obtained suspension in step...
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