Method for removing sodium oxalate from industrial sodium aluminate solution
A technology for industrial sodium aluminate and sodium oxalate, applied in the field of impurity sodium oxalate, can solve the problems of calcium oxalate crystal seed being easy to lose activity, unfavorable sodium oxalate crystallization precipitation, sodium oxalate easy to lose activity, etc., achieving low cost, pretreatment Simple process, easy to separate effects
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[0045] Example 1
[0046] The concentration of caustic alkali in the decomposition mother liquor of an alumina factory is 162g / L. When the concentration of caustic alkali is 243g / L after evaporation and concentration, at a constant temperature of 40℃, 20g / L aluminum hydroxide seed crystals are added, and the rotation speed is 100r / Stir for 12 hours under the condition of min, stop stirring, filter the slurry with a vacuum filter, and return the filtrate to the main production process of Bayer Process. The filter cake is washed with hot water at 60℃ and filtered with a vacuum filter. The composition of the filter cake is hydroxide. Aluminum is used as the seed crystal for the next batch of sodium aluminate solution to crystallize sodium oxalate. The filtrate mainly contains sodium oxalate, and caustic is recovered by causticization. After the above treatment, the sodium oxalate content in the sodium aluminate solution returned to the main production process of the Bayer process de...
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[0047] Example 2
[0048] The concentration of caustic alkali in the decomposition mother liquor of an alumina factory is 162g / L, and when the concentration of caustic alkali is 180g / L after evaporation and concentration, at a constant temperature of 20°C, 10g / L aluminum hydroxide seed crystals are added, and the speed is 100r / Stir for 24 hours under the condition of min, stop stirring, filter the slurry with a vacuum filter, and return the filtrate to the main production process of Bayer Process. The filter cake is washed with hot water at 60℃ and filtered with a vacuum filter. The composition of the filter cake is hydroxide. Aluminum is used as the seed crystal for the next batch of sodium aluminate solution to crystallize sodium oxalate. The filtrate mainly contains sodium oxalate, and caustic is recovered by causticization. After the above treatment, the sodium oxalate content in the sodium aluminate solution returned to the main production process of the Bayer process decrea...
Example Embodiment
[0049] Example 3
[0050] The concentration of caustic alkali in the decomposition mother liquor of an alumina factory is 162g / L, and when the concentration of caustic alkali is 243g / L after evaporation and concentration, at a constant temperature of 35℃, 20g / L aluminum hydroxide seed crystals are added, and the speed is 100r / Stir for 48 hours under the condition of min, stop stirring, filter the slurry with a vacuum filter, and return the filtrate to the main production process of Bayer Process. The filter cake is washed with hot water at 60℃ and filtered with a vacuum filter. The composition of the filter cake is hydroxide. Aluminum is used as the seed crystal for the next batch of sodium aluminate solution to crystallize sodium oxalate. The filtrate mainly contains sodium oxalate, and caustic is recovered by causticization. After the above treatment, the sodium oxalate content in the sodium aluminate solution returned to the main production process of the Bayer process decreas...
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