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Mortar recovery technique for cutting single-crystal and polycrystalline silicon wire

A polysilicon wire and mortar technology, applied in stone processing tools, fine working devices, working accessories, etc., can solve problems such as low efficiency, changes in PEG molecular structure, and decreased quality and efficiency of silicon slices

Inactive Publication Date: 2008-12-24
正申科技(北京)有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0027] ① During the treatment process, only the waste mortar is physically separated, the solid-liquid two phases are not separated, and the recovered product is still black thick mortar;
[0028] ② There are still 10% to 20% solid impurities and tiny particles attached to the surface of SiC particles and suspended in PEG in the system that cannot be completely removed, and these impurities that have not been completely removed will continue to accumulate in the system with the increase in the number of cutting , after a period of time, the quality and efficiency of its recycled products used for silicon slicing have dropped significantly;
[0031] ①Using multi-stage filtration technology for solid-liquid separation, the process is complicated and the efficiency is low;
[0033] ③ The PEG liquid obtained after solid-liquid separation requires a water removal process, which consumes a lot of energy and may also cause changes in the molecular structure of PEG;
[0034] ④ Use water separation technology to classify SiC particles, which has low efficiency and large floor space;
[0035] ⑤ Classify SiC particles first and then chemically treat SiC particles, so that the normal distribution of the final SiC particle size will be shifted again, affecting the effect of silicon slicing

Method used

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  • Mortar recovery technique for cutting single-crystal and polycrystalline silicon wire
  • Mortar recovery technique for cutting single-crystal and polycrystalline silicon wire
  • Mortar recovery technique for cutting single-crystal and polycrystalline silicon wire

Examples

Experimental program
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Effect test

Embodiment 1

[0092] The waste mortar is put into the microporous filter for a membrane filtration solid-liquid separation. After a period of time, when the filter residue wrapping the filter tube (membrane) in the microporous filter accumulates to a certain thickness, due to gravity, it will flow from the filter tube ( The outer wall of the membrane) falls off. At this time, it is necessary to stop feeding, open the slag discharge hole at the bottom of the microporous filter to discharge the filter residue out of the microporous filter; for different mortar processing volumes and different types of microporous filters, the processing time Not all are the same. Practical note: the filtration area is 30m 2 , Filtration speed is 45~65L / m 2 h microporous filter to filter 4 to 8 tons of mortar and complete a separation of membrane filtrate, it takes 2 to 4 hours.

Embodiment 2

[0094] Use a pump to drive the SiC aqueous solution in the pool into the filter press, and perform solid-liquid separation by means of filter press. Filtration area is 125m 2 , There are 48 filter chambers, the filter cake volume is 2m 3 It takes 15-35 minutes to press filter the aqueous solution of 2 tons of SiC solids, and 10-25 minutes to unload; when drying, use an electric rotary drying furnace with a processing capacity of 200kg / h to dry materials containing about 2 tons of SiC , It takes 8 to 10 hours.

Embodiment 3

[0096] Using negative pressure self-distributing gas sorting technology for SiC, it has high precision and high production efficiency, and the classification efficiency can be 250-500kg / h. If 200 tons of SiC are processed per month, calculated on the basis of 16h / day work, only one set is needed. Moreover, it occupies a small area, has high efficiency, and saves labor.

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Abstract

The present invention relates to a technique of recovering mortar used in the wire cutting of monocrystalline silicon or polycrystalline silicon. Silicon is an important material for solar batteries, semiconductors, liquid crystal displays, etc. A silicon rod is cut into silicon wafers by the wire cutting technique, and in the process, a wire-cutting machine needs to be added with cutting liquid mortar, which is mainly composed of liquid phase polyethylene glycol and solid phase silicon carbide powder. When the wire-cutting machine cuts the silicon rod, the solid particles in the mortar are changed into waste mortar as the silicon carbide grinds the silicon rod and a steel wire. If the waste mortar is discharged directly, environment is polluted, and the raw material is wasted. The present invention adopts the mortar-recovering technique to recover the waste mortar, so that the waste mortar can be reused and the discharging of the three wastes can be reduced, so while reducing production cost, the mortar-recovering technique can protect environment. The technique of recovering mortar used in the wire cutting includes the following flow: waste mortar dope, one-step membrane filtration and PEG liquid; waste mortar dope, one-step membrane filtration, cleaning, powder drying, powder classification and SiC powder.

Description

technical field [0001] The invention relates to a technology for recovering mortar used for wire cutting of single crystal and polycrystalline silicon. Silicon is an important material used in solar cells, semiconductors, liquid crystal displays, and more. The application process of silicon materials in the solar energy manufacturing industry is: silicon raw materials→silicon ingots→silicon rods→silicon wafers→polycrystalline silicon cells→solar cell components and application systems; among them, the silicon rods are cut into silicon wafers. The wire cutting machine adds cutting fluid, that is, new mortar, and then discharges the waste mortar, thus, the problem of recycling and reusing the waste mortar is raised. technical background [0002] 1. Description of the composition of the new mortar, the composition of the new mortar and the waste mortar is shown in Table 1: [0003] Polyethylene Glycol, abbreviated as PEG. Molecular formula: HO(CH 2 CH 2 O)nH, the larger n,...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B28D1/02B28D5/00B28D7/00
Inventor 周寿增周正曹孜
Owner 正申科技(北京)有限公司
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