Color filter, process for producing the same, and liquid crystal display device
A manufacturing method and color filter technology, applied in the field of color filters, can solve problems such as narrowing of the effective range and insufficient sensitivity, and achieve the effect of expanding the effective range of development
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Embodiment 1
[0318] (Example 1): coating method
[0319]
[0320] Dissolve 23.1 g of silver (I) acetate, 65.1 g of tin acetate, 54 g of gluconic acid, 45 g of sodium pyrophosphate, 2 g of polyethylene glycol (molecular weight 3000), and E735 (manufactured by ISP, vinylpyrrolidone / vinyl acetate copolymer) 5 g to obtain solution 1.
[0321] Separately, 36.1 g of hydroxyacetone was dissolved in 500 ml of pure water to obtain a solution 2.
[0322] While keeping the solution 1 obtained above at 25° C., while vigorously stirring, the above solution 2 was added thereto within 2 minutes, and stirring was continued slowly for 6 hours. In this way, the mixed liquid changed to black, and silver-tin composite particles were obtained. Then, the liquid was centrifuged to precipitate silver-tin composite particles. The centrifugation was divided into a small amount of 150 ml liquid, and it was carried out for 30 minutes at a rotation speed of 2000 r.p.m using a desktop centrifugal separator H-103n...
Embodiment 2
[0413] The color filter was formed by the method similar to Example 1 except having changed the formulation of the photosensitive resin composition 2 described in said Table 1.
Embodiment 3
[0415]
[0416] Mixed silver particles (major axis length L: 400nm, width b: 30nm, thickness t: 25nm, b / t=1.2) 73.5g, Solspa (Solspa) 20000 (manufactured by Abyssia; dispersion agent) 1.05g, and methyl ethyl ketone 16.4g. This was dispersed using an ultrasonic dispersant (Ultrasonic generator model US-6000ccvp, manufactured by Nissei Co., Ltd.) to obtain a silver microparticle dispersion liquid having a circle-equivalent diameter of 100 nm.
[0417]
[0418] The following compositions were mixed to prepare a photosensitive resin composition.
[0419] 〔composition〕
[0420] ·Silver particle dispersion ...26.1 parts
[0421] ·Propylene glycol monomethyl ether acetate ...28.6 parts
[0422] ·Butanone ...37.6 parts
[0423] 1...0.21 parts of the surfactant
[0424] ·Hydroquinone monomethyl ether ...0.001 parts
[0425]· Benzyl methacrylate / methacrylic acid copolymer ... 2.18 parts
[0426] (Molar ratio=73 / 27, molecular weight 30000)
[0427] Bis[4-[N-[4-(4,6-bistrichlo...
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