Ni-Zn soft magnetic ferrite material and preparation method thereof

A soft ferrite and ferrite material technology, applied in the field of soft ferrite material and its preparation, can solve problems such as failure to develop successfully

Inactive Publication Date: 2009-03-18
广东肇庆微硕电子有限公司 +1
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  • Application Information

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Problems solved by technology

[0002] With the technological upgrading and development of high-tech products such as laptop computers, digital products, LCD TVs, and micro-communications, the demand for nickel-zinc soft ferrite cores is increasing, and tends to be miniaturized, with high reliability and low The direction of production cost development requires stable magnetic permeability, TC, Bm, anti-demolition strength, and high Q, and the nickel-zinc soft ferrite core mainly uses nickelous oxide precious metal as the main raw material, and the addition amount is 10% ~25%. At the same time, as a rare and precious metal, nickel plays an important role in military industry, national defense, and aerospace. It is a strategic resource. Many countries have adopted restrictions on quantitative mining. With the rapid development of the magnetic material industry, nickel The demand is also growing at a high speed, which has caused a t

Method used

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Embodiment

[0012] In a method for preparing a nickel-zinc soft magnetic ferrite material, the steps are: raw material processing, batching, primary ball milling, drying, powdering or sieving, pre-calcination, secondary batching, secondary ball milling, secondary drying, and secondary powdering or sieve, the pre-calcination condition is pre-synthesis in an air furnace at 900-980°C, and the sintering temperature is 1050-1100°C. The said pre-sintering time is 2 hours, and the said sintering time is 3 hours. In the above steps, the Fe 2 o 3 . 2 o 3 , CO 2 o 3 , Mn 3 o 4 、CaCo 3 . The performance test parameters of the finally obtained nickel-zinc soft magnetic ferrite material are shown in Table 2 corresponding to material formulations 1-13. That is, the obtained nickel-zinc soft magnetic ferrite material has high Q, high-frequency characteristics, high TC, Bm, and low cost.

[0013] Table 1: Formula of Ni-Zn soft ferrite material

[0014] Recipe

[0015] Table 2: Perfo...

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Abstract

The invention discloses a nickel-zinc soft magnetic ferrite material and a preparation method thereof. The material comprises the following compositions in mol percentage: 45 to 50 mol percent of ferric oxide Fe2O3, 20 to 26 mol percent of zinc oxide ZnO, 12 to 17 mol percent of nickel protoxide NiO, 5 to 10 mol percent of copper oxide CuO, and 3 to 10 mol percent of magnesium oxide MgO. The preparation method comprises the following steps: treating raw materials, proportioning, primary ball milling, drying, powdering or screening, preburning, secondary proportioning, secondary ball milling, secondary drying and secondary powdering or screening; the preburning condition is to carry out pre-synthesis in an air furnace at a temperature of between 900 and 980 DEG C, and the sintering temperature is between 1,050 and 1,100 DEG C. The nickel-zinc soft magnetic ferrite material has the characteristics of property of high Q, high frequency, high TC, high Bm and low cost.

Description

technical field [0001] The invention relates to a soft ferrite material and a preparation method thereof, in particular to a nickel-zinc soft ferrite material and a preparation method thereof. Background technique [0002] With the technological upgrading and development of high-tech products such as laptop computers, digital products, LCD TVs, and micro-communications, the demand for nickel-zinc soft ferrite cores is increasing, and tends to be miniaturized, with high reliability and low The direction of production cost development requires stable magnetic permeability, TC, Bm, anti-demolition strength, and high Q, and the nickel-zinc soft ferrite core mainly uses nickelous oxide precious metal as the main raw material, and the addition amount is 10% ~25%. At the same time, as a rare and precious metal, nickel plays an important role in military industry, national defense, and aerospace. It is a strategic resource. Many countries have adopted restrictions on quantitative mi...

Claims

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Application Information

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IPC IPC(8): C04B35/26
Inventor 李刘清王国华李际勇胡满明龚锋刘小红韦建军王灿飞梁均林黄燕军陈武气
Owner 广东肇庆微硕电子有限公司
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