Technique for producing edible ethyle ester type chrysalis oil using chrysalis crude-oil

A technology of grade ethyl ester and silkworm chrysalis oil, applied in the directions of edible oil/fat, application, food preparation, etc., can solve the problems of high acid value and peroxide value, unpleasant fishy odor, etc., and achieve high product quality and good sensory indicators , complete deodorization effect

Inactive Publication Date: 2009-04-01
景凯
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] Silkworm chrysalis oil contains a variety of unsaturated fatty acids, the content of which is as high as 75%, of which the content of α-linolenic acid is more than 30%, the content of linoleic acid is about 7%, and the content of oleic acid is about 32%. It is worth mentioning that silkworm chrysalis oil It also contains a certain amount of odd-numbered carbon fatty acids C15 and C17. During the development of anticancer drugs, Dr. Mitsuhiro Numata found that odd-numbered carbon fatty acids have high anticancer activity, and odd-numbered carbon fatty acids are extremely important in land organisms. It is rare, which makes silkworm chrysalis oil valuable for development and utilization; the silkworm chrysalis hair oil that is usually extracted by solvent or mechanically squeezed and separated is dark brown in color, high in acid value and peroxide value, and has an unpleasant fishy smell

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment

[0019] (1) Degumming: Take 100 kg of silkworm chrysalis hair oil that has been extracted by organic solvents or mechanically squeezed and separated, heat it to 65--80 °C, add 0.2 kg of food-grade phosphoric acid with a concentration of 85%, and then add 70-90 °C 4 kg of hot water, stir for 15-25 minutes, stand for separation or pump into the separator for separation and degumming;

[0020] (2) Dehydration: Carry out vacuum dehydration to the feed liquid after degumming, the vacuum degree is a negative pressure of 0.05-0.15MPa, and the temperature is 90-98°C;

[0021] (3) Esterification: Add 80 kilograms of dehydrated ethanol and 3 kilograms of concentrated sulfuric acid with a concentration of 98% to the feed liquid after degumming and dehydration, and heat and reflux for transesterification. The transesterification temperature is 65-75° C. 5--6 hours;

[0022] (4) reclaim ethanol: after esterification is finished, distillation reclaims the ethanol of 70-75% of feed intake, a...

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Abstract

The invention discloses a process used for producing edible ethyl ester-typed silkworm pupa oil by silkworm pupa crude oil, comprising the main steps as follows: silkworm pupa crude oil extracted by organic solvent or squeezed and separated by machines is degummed, dehydrated and esterified; ethanol is recovered, glycerin and sulphuric acid are separated and washed; saturated fatty acids are removed and distilled; during the distillation process, the distillate with the temperature of 120-140 DEG C and the pressure of 1-5Pa is intercepted. The ethyl ester-typed edible silkworm oil produced by the process has good sensory index and the color thereof is buff; no crystals occur at zero DEG C; unsaturated fatty acid has high content; the acid value and peroxide value of the oil reach the edible standard, the quality of the product is good, the safety is high and no solvent remains; the process can be widely applied to the industries such as medicines, health-caring food, nutrition food, high-grade cosmetics and the like.

Description

technical field [0001] The invention belongs to the technical field of production technology of edible grade silkworm chrysalis oil technical background [0002] Silkworm chrysalis oil contains a variety of unsaturated fatty acids, the content of which is as high as 75%, of which the content of α-linolenic acid is more than 30%, the content of linoleic acid is about 7%, and the content of oleic acid is about 32%. It is worth mentioning that silkworm chrysalis oil It also contains a certain amount of odd-numbered carbon fatty acids C15 and C17. During the development of anticancer drugs, Dr. Mitsuhiro Numata found that odd-numbered carbon fatty acids have high anticancer activity, and odd-numbered carbon fatty acids are extremely important in land organisms. It is rare, which makes silkworm chrysalis oil valuable for development and utilization; the silkworm chrysalis crude oil that is commonly extracted by solvents or mechanically squeezed and separated is dark brown in colo...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A23D9/04A23L1/29A23L1/015A23L1/277A23L5/20A23L5/49A23L33/00
Inventor 景凯
Owner 景凯
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