Sialon complex phase ceramic lift tube and production method thereof
A technology of composite ceramics and riser tubes, which is applied in the field of ceramic materials and preparation of riser tubes, can solve the problems of online service life of only ten days, no mass production, oxidation-reduction reaction, etc., and achieve stable and reliable product performance, Easy to operate, simple process effect
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Embodiment 1
[0010] Embodiment 1, the composition of the raw materials of the multiphase ceramic riser and the percentages by weight of various raw materials are: 35% silicon nitride, 20% quartz, 14% aluminum dioxide, 0.05% yttrium oxide, 25% silicon carbide, zirconia 5.2%, acrylamide 0.048%, N,N'-methylenebisacrylamide 0.002%, polymethacrylamine 0.6%, persulfate ammonium 0.1%.
Embodiment 2
[0011] Embodiment 2, the raw material composition of the multiphase ceramic riser and the weight percentages of various raw materials are: silicon nitride 40%, quartz 18%, aluminum dioxide 10%, yttrium oxide 0.05, silicon carbide 25, zirconia 6.2% , Acrylamide 0.048%, N, N'-methylenebisacrylamide 0.002%, polymethacrylic acid amine 0.6%, persulfate amine 0.1%.
[0012] On the basis of the above-mentioned raw material ratio, the ceramic liquid riser with higher performance can be produced by using the existing preparation method through the processes of wet ball milling, injection molding, curing, mold releasing, drying and firing.
Embodiment 3
[0013] Example 3, for the raw material composition of Example 1, the preparation method of the multi-phase ceramic riser is to adopt the near-net size injection molding process, and go through the wet ball milling, injection molding, curing, demoulding, drying and firing processes be made of. Among them: wet ball milling is to add deionized water, acrylamide and N, N'-methylenebisacrylamide in the ball mill in advance as a premixed solution, wherein the amount of deionized water added accounts for 30% by weight of all raw materials, and then Add silicon nitride, quartz and yttrium oxide and ball mill for 3-5 hours, then add aluminum dioxide, silicon carbide and zirconia for ball milling, the total time of ball milling is 15-30 hours. The particle size detected after grinding is <3.0 microns. Injection molding is to put the ball-milled slurry into a vacuum mixer, add ammonium persulfate, vacuumize, remove the gas, and then use a vacuum mixer to inject it into the mold under a ...
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