High temperature resistant, high strength modified epoxy resin adhesive and preparation thereof
An epoxy resin, high-strength technology, applied in the direction of epoxy resin glue, adhesive, adhesive type, etc., can solve the problems of brittleness and poor temperature resistance, and achieve excellent high temperature resistance, outstanding heat resistance, excellent The effect of high temperature resistance
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[0032] Examples:
[0033] Preparation of polyurethane prepolymer: The polyether glycol used has a number average molecular weight of 1,000. Add 50g of polyether glycol into a clean and dry four-necked flask, heat and continue stirring to 120°C for reflux dehydration for 1 hour, then cool it to 50°C, add 17.4g of TDI, and then slowly raise the temperature to 70°C, keep warm Stir at a constant speed and react for 2 hours.
[0034] Adhesive configuration: add 1.68g 1,4-butanediol and 0.56g trimethylolpropane to the prepared polyurethane prepolymer, mix well and then add 366.5g TDE-85 and E-51 to mix (mass ratio In the epoxy resin of 1:1), react at 100°C for 1 hour. Take 54.52g each of m-phenylenediamine and diaminodiphenylmethane, mix them uniformly in a beaker, keep them at 110°C for 15 minutes, and cool to room temperature to prepare supercooled liquid. Finally, the supercooled liquid is mixed with polyurethane epoxy resin at room temperature, and 13.08g of 2-ethyl-4-methylimidazol...
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