Method for producing sugar charcoal particle sugar charcoal by physical method
A production method and technology of physical method, applied in the production field of physical method granular sugar charcoal, can solve the problems of frequent regeneration, short operation period, poor use effect, etc., and achieve the effect of good caramel decolorization and high wear resistance
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Embodiment 1
[0024] Embodiment 1 utilizes anthracite to produce granular sugar charcoal
[0025] 1. Add 120g of ammonium polyphosphate and 300g of petroleum hard asphalt to 2000g of anthracite, crush them together to 200 mesh, then add 500g of coal tar, and then add 200ml of sodium hydroxide and sodium phosphate aqueous solution with a concentration of 15% after kneading to form a certain Blend of softness.
[0026] 2. Put the above mixture at 200kg / cm 2 Under pressure, it is extruded into a columnar strip through a metal mold with a hole diameter of φ2mm~φ4mm.
[0027] 3. After drying the columnar strips, put them into the carbonization furnace. The carbonization furnace uses electric heating wire to heat slowly under the condition of isolating the air. The heating rate is maintained at 5°C to 10°C / min. When the temperature rises to 500°C to 550°C, keep it at a constant temperature for half an hour for carbonization, so that the strips out of the furnace become carbonized materials. ...
Embodiment 2
[0033] Embodiment 2 utilizes anthracite to produce granular sugar charcoal (do not use ammonium polyphosphate)
[0034] Add 300g of petroleum hard asphalt to 2000g of anthracite, pulverize together to 200 mesh, then add 500g of coal tar, knead and then add 200ml of sodium hydroxide and sodium phosphate aqueous solution with a concentration of 15% and knead at 200kg / cm 2 Extrude into columnar strips under pressure, carbonize at 500°C-550°C for half an hour, extrude into columnar strips, activate the carbonized material in the activation furnace after drying, and pass in superheated water at 450°C when the temperature rises to 750°C Steam, the activation temperature is controlled between 920°C and 950°C, and the activation time is 5.5 hours. 740 g of granular sugar charcoal was obtained. The technical indicators of the assay are:
[0035] Iodine adsorption value
[0036] Embodiment 2 illustrates: if the present invention does not use ammonium polyphosphate, only use ...
Embodiment 3
[0037] Embodiment 3 Utilizes non-caking bituminous coal to produce granular sugar charcoal
[0038] Add 160g of ammonium polyphosphate and 280g of petroleum hard asphalt to 2000g of non-caking bituminous coal, grind them together to 250 mesh, then add 400g of coal tar, knead, and then add 20% sodium hydroxide and 200ml of sodium dihydrogen phosphate aqueous solution to knead , at 180kg / cm 2 Extrude into columnar strips under pressure, and carbonize at 500°C to 550°C. After drying, the carbonized material is activated in the activation furnace. When the temperature rises to 750°C, superheated steam at 450°C is introduced. 920°C, activation time 4.5 hours. 685 g of granular sugar charcoal was obtained.
[0039] The technical indicators of the assay are:
[0040] Iodine adsorption value
[0041] 965mg / g
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