Method for producing red iron oxide pigment

A technology of iron oxide red and production method, which is applied in the direction of iron oxide, iron oxide/iron hydroxide, etc., can solve the problems of long production cycle, high production cost, complicated process, etc., and achieve short production process, stable product quality and excellent process Easy-to-grasp effects

Inactive Publication Date: 2009-09-30
NINGBO RONBAY LITHIUM BATTERY MATERIAL CO LTD
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Problems solved by technology

[0007] In order to overcome the above-mentioned deficiencies, the purpose of the present invention is to provide a production method of iron oxide red pigment in the art, so that it can solve the problem of high energy consumption, long production cycle, complicated process and high production cost of existing similar products. relatively high technical issues

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  • Method for producing red iron oxide pigment

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[0017] The implementation mode takes actual production as an example. at 10m 3 Inject about 5m into the plastic reactor 3 of water, start stirring, throw in 1500Kg of jarosite slag after removing iron in the cobalt chloride hydrometallurgy process, control the pH at 5-6, dehydrate the jarosite slag through a plate-and-frame filter press after half an hour, and make the water content Control it below 40%. Drying is carried out by a drying tunnel kiln, which is equipped with a liquefied gas delivery system; then the alum slag filter cake is loaded into a porcelain boat, and sent to the drying tunnel kiln for 3 to 5 hours, with the temperature controlled at 120 to 150 °C. The iron slag is cooled, pulverized by a pulverizer, put into a mullite bowl, sent to a calciner for calcination for 2-4 hours, and the calcination temperature is controlled at 550-650°C. The calcined powder is put into a plastic reactor, washed with water at 60-90°C, stirred for half an hour, dehydrated into...

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Abstract

The invention relates to a method for producing a red iron oxide pigment. The method has the main points: adding water into waste iron vitriol dregs for coarse washing, dewatering the waste iron vitriol dregs with a frame filter press, placing the dewatered waste iron vitriol dregs in a drying oven for drying at 120 to 150 DEG C for 3 to 5 hours; and cooling the iron vitriol dregs, crushing the cooled iron vitriol dregs and filling the crushed iron vitriol dregs in a porcelain boat, placing the crushed iron vitriol dregs in a high temperature calciner for calcination treatment at a temperature of 550 to 650 DEG C for 2 to 4 hours, absorbing furnace tail gas SO3 with 60 percent sulfuric acid to produce more than or equal to 98 percent concentrated sulfuric acid, and absorbing residual air after absorption with sodium hudroxide. Powder formed by calcining the iron vitriol dregs is washed, and the temperature is controlled to be 60 to 90 DEG C; after being washed, the powder is dewatered by the frame filter press and then enters the drying oven to be dried at a low temperature of 120 to 150 DEG C for 2 to 3 hours; and the dried powder is passed through a 150 mesh sieve to obtain a finished product of the red iron oxide pigment. The method emphasizes environmental protection in a production process and has the characteristics of low energy consumption, short production flow, easy mastered process, stable product quality, change of waste into valuable, and the like.

Description

technical field [0001] The invention relates to a production method of chemical products, in particular to a method for producing red iron oxide pigments from waste ferrite slag as a raw material. Background technique [0002] Iron oxide red is widely used in colored bricks and tiles, colored cement, architectural coatings and paints, inks and other industries. At present, the production of high-purity iron oxide red in my country mostly uses high-purity low-carbon steel flakes or finished high-priced iron salts as raw materials. It is difficult to collect such raw materials, the source is uncertain, the price is relatively expensive, and the quantity is very small. There are also some iron oxide red production methods that use iron-containing industrial waste residue, slag, iron mud, etc. as raw materials. Most of these methods need to go through acid-dissolving, magnetic separation and other treatment processes, and the production process is long and energy-consuming. [...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C01G49/06
Inventor 沈恒冠袁巧平韩道洋
Owner NINGBO RONBAY LITHIUM BATTERY MATERIAL CO LTD
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