Alpha-Fe2O3 bowl-shaped photon crystal structure and preparation method thereof
A technology of photonic crystals and crystal structures, which is applied in crystal growth, microsphere preparation, chemical instruments and methods, etc., can solve problems affecting the application quality of nanomaterials, nano-iron oxide dispersion, etc., and achieve lower equipment requirements and good repeatability , low cost effect
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Embodiment 1
[0018] a), making a single-layer polystyrene ball template
[0019] Clean the silicon wafer, put it vertically into the suspension of polystyrene beads with a mass fraction of 0.1% after being ultrasonicated for 3 hours, then put it in an electric constant temperature blast drying oven for 3 days at a temperature of 40°C to obtain a single layer Polystyrene pellet template.
[0020] b) Growth of α-Fe 2 o 3 Two-dimensional bowl-shaped photonic crystal structure
[0021] Put the template obtained in step a into a vacuum chamber for 3 minutes, the vacuum degree is 3Pa; configure 1.5mol / L FeNO 3 water solution, and take one drop of the solution and drop it on the template; place the template in an electric constant temperature blast drying oven for 3 hours at a temperature of 110°C, and at this time FeNO 3 The aqueous solution was evaporated to dryness and transformed into α-Fe 2 o 3 Two-dimensional bowl-shaped photonic crystal structure.
[0022] c), remove the polystyrene...
Embodiment 2
[0025] a), making a single-layer polystyrene ball template
[0026] Clean the silicon wafer, put it vertically into the suspension of polystyrene beads with a mass fraction of 0.2% after being ultrasonicated for 3 hours, then put it into an electric constant temperature blast drying oven for 4 days at a temperature of 50°C to obtain a single layer Polystyrene pellet template.
[0027] b) Growth of α-Fe 2 o 3 Two-dimensional bowl-shaped photonic crystal structure
[0028] Put the template obtained in step a into a vacuum chamber for 2 minutes, the vacuum degree is 4Pa; configure 1mol / L FeNO 3 water solution, and take one drop of the solution and drop it on the template; place the template in an electric constant temperature blast drying oven for 2 hours at a temperature of 150°C, and at this time FeNO 3 The aqueous solution was evaporated to dryness and transformed into α-Fe 2 o 3 Two-dimensional bowl-shaped photonic crystal structure.
[0029] c), remove the polystyrene...
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