Amorphophallus glucomannan drying agent and preparation method thereof

A technology of konjac glucomannan and glucomannan, applied in chemical instruments and methods, other chemical processes, etc., can solve the problem that konjac super absorbent is not suitable for low-humidity environment, konjac glucomannan swells slowly, polymer The problem of high price of water absorbent

Inactive Publication Date: 2010-03-17
FUJIAN AGRI & FORESTRY UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

However, due to their own shortcomings, such as the low water absorption capacity of silica gel, the water absorption can easily reach saturation at high humidity; quicklime gradually becomes an aqueous solution during the moisture absorption process; Wide application in fields such as
[0005] In the "Study on the Hygroscopic Properties of Konjac Glucomannan-Acrylic Acid Graft Copolymer" published in "Journal of Agricultural Engineering", Li Wanfen and others proposed to use konjac glucomannan as raw material and acrylic acid graft modification to synthesize konjac super absorbent agent , has strong water absorption, and also has hygroscopicity, but the swelling of konjac glucomannan is slightly slower, and konjac super absorbent is not suitable for use in low humidity environment

Method used

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Embodiment Construction

[0013] In order to fully disclose the konjac glucomannan desiccant of the present invention and its preparation method, the following examples will be used to illustrate.

[0014] The preparation method of konjac glucomannan desiccant of the present invention consists of the following steps:

[0015] (1) Preparation of deacetylated konjac glucomannan: bake 20 g of konjac glucomannan at 60°C for 3 hours, mix with 0.4 g of sodium hydroxide, put the mixture in the grinding cylinder of a dry vibrating mill, and carry out deacetylation for 25 minutes. After the acetyl modification treatment, immerse the modified product in 100ml of 50% (V / V) ethanol solution for 5min; then neutralize to pH=7 with 6mol / L HCl solution, and then use 50% (V / V) ) was washed with ethanol solution 3 times, each time for 30 min, while stirring, and the stirring speed was 400r / min; after 3 times of washing, vacuum filtration was performed under the condition of 0.7Mpa until the supernatant liquid of suction...

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Abstract

The invention relates to an amorphophallus glucomannan drying agent which consists of amorphophallus glucomannan, propenoic acid, sodium hydroxide, ethanol, hydrochloric acid, potassium persulfate, N,N-methylene-bisacrylamide, calcium chloride and water. The preparation method of the drying agent comprises the steps of: preparing deacetylation amorphophallus glucomannan and deacetylation amorphophallus glucomannan-propenoic acid copolymer; mixing the deacetylation amorphophallus glucomannan and the deacetylation amorphophallus glucomannan-propenoic acid copolymer according to a proportion; andcrushing and pelleting after expansion. The drying agent has the advantages of reasonable formula, low cost, strong water absorption, safety, no toxicity, no harm to skin and eyes, biodegradability and the like, and can be widely applied to the fields such as food, medicine, chemical industry and the like.

Description

technical field [0001] The invention relates to a desiccant and a preparation method thereof, in particular to a konjac glucomannan desiccant with konjac glucomannan as a main raw material and a preparation method thereof. Background technique [0002] In view of the traditional desiccant, silica gel, quicklime, molecular sieve and polymer water-absorbing agent are often used as the main raw materials. However, due to their own shortcomings, such as the low water absorption capacity of silica gel, the water absorption can easily reach saturation at high humidity; quicklime gradually becomes an aqueous solution during the moisture absorption process; Wide application in other fields. Therefore, the research of a new type of desiccant has attracted much attention, especially the edible desiccant has become one of the hot spots in the development of the desiccant manufacturing industry. The new generation of desiccants use natural materials as raw materials, which can be divi...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01J20/30C08F251/00C08B37/00
Inventor 庞杰吴春华庄昱温成荣曾援
Owner FUJIAN AGRI & FORESTRY UNIV
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