Polycaprolactone metal fiber
A polycaprolactone and metal fiber technology, applied in the direction of single-component polyester rayon, yarn, textiles and papermaking, can solve the problems of limited processing and application, low strength, and difficult synthesis of high molecular weight polyester. Achieve the effect of improving mechanical strength and soft hand feeling
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[0014] First synthesize high-molecular-weight polycaprolactone: the raw material is caprolactone, the catalyst is sodium silicate and tetrabutyl titanate, and the amount of sodium silicate added is 150×10 of the amount of butanediol. -6 , the amount of tetrabutyl titanate added is 400×10 of the amount of butanediol -6 . Sodium silicate, tetrabutyl titanate, flame retardant, matting agent and caprolactone are mixed into a slurry and enter the first reactor, and the stabilizer is added into the fourth reactor in the final reaction stage. The continuous polymerization process is completed through four reactors. The synthesis process of polycaprolactone:
[0015] condition
Reactor I
Reactor II
Reactor III
Reactor IV
140~150
160~180
200~210
200~210
Reaction pressure / Pa
(1.3~1.5)×10 5
6.0×10 4
2500~3000
50~100
Residence time / min
60~90
60~90
50~70
120~...
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