Acid soaping agent
A soaping agent and acid technology, applied in the field of printing and dyeing auxiliaries, can solve the problem of wasting water resources, and achieve the effects of excellent anti-staining performance, excellent washing fastness and anti-staining performance, and shortening the process flow.
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Embodiment 1
[0014] Add 72 grams of acrylic acid and 470 grams of lauryl alcohol polyoxyethylene (9) ether into a 2000ml four-necked flask equipped with a reflux condenser, start stirring, blow nitrogen, heat up to 135°C, and keep warm at 135-140°C for reaction After 3.5-4.0 hours, the temperature is lowered, the material is discharged, and a polymerized monomer with surface activity is synthesized.
Embodiment 2
[0016] Take 12 grams of polymerized monomers, 2 grams of maleic anhydride, and 40 grams of deionized water in Example 1 and add them to a four-neck flask, stir, blow nitrogen, heat up to 70°C, add 0.05 grams of potassium persulfate, and heat the mixture at 75-80°C After 30 minutes of reaction, add dropwise a mixture of 13 grams of acrylic acid, 3 grams of AMPS, 0.07 grams of potassium persulfate, and 30 grams of deionized water. The dropping time is controlled between 1.5-2.0 hours. After completion, the reaction was continued for 1 hour, the temperature was lowered, and the material was discharged. Take 51 grams of the prepared sample and compound it with 17 grams of fatty amine polyoxyethylene ether (1815), stir evenly, and prepare soaping agent 1#.
Embodiment 3
[0018] Take 10 grams of the polymerizable monomer in Example 1, 10 grams of maleic acid, and 40 grams of deionized water and add them to a four-necked flask, stir, blow nitrogen, heat up to 70 ° C, add 0.06 grams of azobisisobutyronitrile, Insulation reaction at -80°C, after reaction for 30 minutes, add dropwise a mixture of 8 grams of acrylic acid, 2 grams of AMPS, 0.07 grams of ammonium persulfate, and 30 grams of deionized water, and the dropping time is controlled between 1.5-2.0 hours , after the dropwise addition was completed, the reaction was continued for 30 minutes, the temperature was lowered, and the material was discharged. Get 48 grams of the obtained sample and compound with 8 grams of coconut oil diethanolamide (6501), stir well, and make soaping agent 2#.
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