Graphene/conductive polymer composite film and preparation method thereof
A conductive polymer and graphene technology, which is applied in the direction of non-metallic conductors, organic material conductors, carbon-silicon compound conductors, etc., can solve the problems of limited applications, achieve great convenience, simple preparation method conditions, and good electrical conductivity.
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Embodiment 1
[0029] 1) Prepare graphite oxide according to the method reported in the literature (Composites Science and Technology, 2009, 69, 1231);
[0030] 2) in the dilute hydrochloric acid solution containing 1mmol of aniline, adding the ammonium persulfate of 1mmol is an oxidant to prepare polyaniline;
[0031] 3) The graphite oxide and polyaniline obtained in steps 1) and 2) were ultrasonically dispersed in N-methylpyrrolidone for 60 minutes according to a mass ratio of 10:90, 0.2g of hydrazine hydrate was added thereto, and stirred for 24 hours;
[0032] 4) Add the above solution dropwise to the substrate rotating at 3000 rpm, spin coating for 30 seconds, wash and dry;
[0033] 5) Repeat step 4) and cycle 100 times to obtain a graphene / polyaniline composite film with a film thickness of about 1 μm and an electrical conductivity of 2×10 -2 S / cm.
Embodiment 2
[0035] 1) Prepare graphite oxide according to the method reported in the literature (Composites Science and Technology, 2009, 69, 1231);
[0036] 2) in the dilute sulfuric acid solution containing 2mmol o-methoxyaniline, adding the ammonium persulfate of 2mmol is an oxidant to prepare poly-o-methoxyaniline;
[0037] 3) The graphite oxide and poly-o-methoxyaniline obtained in steps 1) and 2) were ultrasonically dispersed in N-methylpyrrolidone for 60 minutes according to a mass ratio of 30:70, 0.4 g of hydrazine was added thereto, and stirred for 36 hours ;
[0038] 4) Immerse the substrate in the above solution, pull out after 5 seconds, wash and dry;
[0039] 5) Step 4) is repeated, and the graphene / poly-o-methoxyaniline composite film is obtained after 5 cycles, the film thickness is about 100 μm, and the conductivity of the composite film is 4×10 -1 S / cm.
Embodiment 3
[0041] 1) Prepare graphite oxide according to the method reported in the literature (Composites Science and Technology, 2009, 69, 1231);
[0042] 2) in the dilute acetic acid solution containing 5mmol 2,5-dimethoxyaniline, adding 5mmol of ammonium persulfate is an oxidant to prepare poly-2,5-dimethoxyaniline;
[0043] 3) The graphite oxide and poly-2,5-dimethoxyaniline obtained in steps 1) and 2) were ultrasonically dispersed in N-methylpyrrolidone for 90 minutes in a mass ratio of 50:50, and 0.2 g of dimethoxyaniline was added thereto. Methylhydrazine, stirred for 48 hours;
[0044] 4) Add the above solution dropwise to the substrate rotating at 3000 rpm, spin coating for 30 seconds, wash and dry;
[0045] 5) Repeat step 4) and cycle 500 times to obtain a graphene / poly-2,5-dimethoxyaniline composite film, the film thickness is about 6 μm, and the conductivity of the composite film is 7×10 1 S / cm.
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