Method for extracting grease from artemia or artemia eggs

A technology for extracting oil and Artemia eggs, which is applied in the direction of fat oil/fat production and fat generation, can solve the problems of accelerating the oxidation of unsaturated fatty acids, difficulty in scaling up, and low oil yield, so as to achieve easy scale-up production and save recycling costs , fast drying effect

Inactive Publication Date: 2012-03-28
天津强微特生物科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Among them, supercritical fluid extraction is a new type of extraction and separation technology developed in recent years. It can be operated at low temperature, avoiding the oxidation and decomposition of unstable unsaturated fatty acids, and there is no residual solvent, CO 2 Easy to obtain, low energy consumption, and has obvious advantages incomparable with other methods. At present, there is no application research report on supercritical extraction in artemia resource oils
And because this method has requirements on the moisture content of the extracted sample, the drying process will be adopted in the supercritical liquid extraction method. At present, direct heating and drying and first freezing and then vacuum drying are mainly used, but direct heating and drying are easy to accelerate. Oxidation of unsaturated fatty acids, first freezing and then vacuum drying scale is not easy to expand and consumes a lot of energy; therefore, the yield of oil obtained is low
In addition, there is a requirement for the moisture in the oil in the process of capsules and other products. The current dehydration methods for oil mainly include drying in an oven, drying with a desiccant such as anhydrous sodium sulfate, and ordinary vacuum drying. There are some shortcomings such as easy to oxidize, not easy to enlarge, and the time is too long.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] 1) Pretreatment of Artemia

[0024] After the artemia that has been selected to remove impurities is quickly soaked and rinsed in the pool, it is fished out with a 100-mesh sieve and placed on the sieve bed until no water drips, and then sent to a vacuum drum double-cone drier. Carry out drying, rotating speed 7r / min, measure sample drying weight loss at intervals, dry to stop under 5% water content in Artemia, then Artemia is pulverized into the powder that passes 120 mesh screens with pulverizer.

[0025] 2) Supercritical extraction of Artemia oil

[0026] Weigh 20Kg of the pretreated raw material, put it into a supercritical extraction kettle, the extraction pressure is 30MPa, the extraction temperature is 35°C, the separation pressure is 15MPa, the separation temperature is 45°C, CO 2 The flow rate is controlled at 200L / h, the extraction time is 120min, and 2.0Kg of oil is obtained.

[0027] 3) Artemia oil refining

[0028] in CO 2 In the supercritically extract...

Embodiment 2

[0030] 1) Pretreatment of Artemia eggs

[0031] The artemia eggs that have been selected to remove impurities are quickly soaked and rinsed in the pool, then fished out with a 100-mesh screen and placed on the sieve bed until no water drips, then sent to a vacuum drum double-cone dryer, at a temperature of 55 ° C. Dry at 6r / min at a rotating speed of 6r / min, take samples at intervals to measure the weight loss on drying of the sample, and dry until the water content in the Artemia ovum stops below 5%, and then the Artemia ovum is pulverized into powder passing through a 140-mesh sieve with a pulverizer.

[0032] 2) Supercritical extraction of Artemia egg oil

[0033] Weigh 40Kg of the pretreated raw material, put it into a supercritical extraction kettle, the extraction pressure is 35MPa, the extraction temperature is 35°C, the separation pressure is 15MPa, the separation temperature is 45°C, CO 2 The flow rate is controlled at 400L / h, the extraction time is 180min, and 7.8Kg...

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PUM

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Abstract

The invention provides a method for extracting grease from artemia or artemia eggs. In the method, a finished product of the grease is obtained by a plurality of steps of preprocessing the artemia or the artemia eggs, carrying out supercritical extraction, refining the grease and the like. Compared with a traditional method, the invention has the characteristics of low-temperature operation, little possibility of oxidation of unsaturated fatty acid, good quality, high yield of the extracted grease, no adoption of an organic solvent in the entire process, high-temperature operation avoidance, combined single-step operation of a plurality of procedures, low energy consumption, easy amplified production and the like.

Description

technical field [0001] The invention relates to a method for extracting oil, in particular to a method for extracting oil from Artemia or Artemia eggs. Background technique [0002] Artemia (Brine Shrimp) is also called Saltwater Artemia, and Chinese folks call it Saltworm or Artemia Shrimp. It belongs to the Arthropoda phylum in classification, with subphylum Gillia, Crustacea, Subclass Branchiopoda, no order, Saltwater Artemia family, Artemia. Artemia and Artemia eggs are rich in protein, amino acids, saturated fatty acids, unsaturated fatty acids and inorganic elements. Therefore, extracting oil from Artemia or Artemia eggs to prepare feed, food and medicine has become a research topic for Artemia. new direction of development. [0003] In the existing oil extraction process, mechanical pressing method, solvent extraction method, supercritical fluid extraction method and biological enzyme method are usually used. Among them, supercritical fluid extraction is a new type...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C11B1/02C11B1/10
Inventor 魏国祥郑春阳原素英
Owner 天津强微特生物科技有限公司
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