Process for producing electroconductive inorganic oxide particles and electroconductive inorganic oxide particles produced by the process
An inorganic oxide, conductive technology, applied in the field of conductive inorganic oxide particles, can solve the problems of not being able to provide cheap products to the market, reduce manufacturing costs, etc., achieve good electrical conductivity, simple composition, and improved purity
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Embodiment 1
[0099] In this example, the aluminum component (Al 3+ ) was doped with zinc oxide (ZnO) particles (CP-1) manufactured by Ishihara Sangyo Co., Ltd. Here, using figure 1 The electrolytic doping device 1 shown. The electrolytic doping device 1 is composed of an electrolytic cell 2 , an anode electrode 3 (aluminum electrode), a cathode electrode 4 (aluminum electrode), a stirring unit 5 , and an external power source 6 . In addition, aluminum plates of 6.0 cm×6.0 cm were used for both the anode electrode 3 and the cathode electrode 4 , and the electrode distance between the anode electrode 3 and the cathode electrode 4 was 3.0 cm. Each step will be described below.
[0100] Step A: Put 400 ml of ion-exchanged water in the electrolytic cell 2 of the electrolytic doping device 1, and add 10 g of zinc oxide powder as inorganic oxide particles and zinc chloride (ZnCl 2 ) 0.05 g, stirred by the stirring unit 5 to prepare a slurry 7 containing zinc oxide particles. In addition, the...
Embodiment 2
[0109] In this example, the gallium component (Ga 3+ ) was doped with zinc oxide (ZnO) particles (CP-1) manufactured by Ishihara Sangyo Co., Ltd. Here, using figure 1The electrolytic doping device 1 shown. The electrolytic doping device 1 is composed of an electrolytic cell 2 , an anode electrode 3 (gallium electrode), a cathode electrode 4 (copper electrode), a stirring unit 5 , and an external power source 6 . In addition, copper plates of 6.0 cm×6.0 cm were used for both the anode electrode 3 and the cathode electrode 4 , and the electrode pitch between the anode electrode 3 and the cathode electrode 4 was set to 3.0 cm. Each step will be described below.
[0110] Step A: Put 400 ml of ion-exchanged water in the electrolytic cell 2 of the electrolytic doping device 1, and add 10 g of zinc oxide powder as inorganic oxide particles and zinc chloride (ZnCl 2 ) 0.05 g, stirred by the stirring unit 5 to prepare a slurry 7 containing zinc oxide particles. In addition, the zi...
Embodiment 3
[0119] In this example, the iridium component (Ir 3+ ) was doped with zinc oxide (ZnO) particles (CP-1) manufactured by Ishihara Sangyo Co., Ltd. Here, using figure 1 The electrolytic doping device 1 shown. The electrolytic doping device 1 is composed of an electrolytic cell 2 , an anode electrode 3 (iridium electrode), a cathode electrode 4 (copper electrode), a stirring unit 5 , and an external power source 6 . In addition, copper plates of 6.0 cm×6.0 cm were used for both the anode electrode 3 and the cathode electrode 4 , and the electrode pitch between the anode electrode 3 and the cathode electrode 4 was set to 3.0 cm. Each step will be described below.
[0120] Step A: Put 400 ml of ion-exchanged water in the electrolytic cell 2 of the electrolytic doping device 1, and add 10 g of zinc oxide powder as inorganic oxide particles and zinc chloride (ZnCl 2 ) 0.05 g, stirred by the stirring unit 5 to prepare a slurry 7 containing zinc oxide particles. In addition, the z...
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Abstract
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