Method for preparing dye-sensitized solar cell

A solar cell and dye sensitization technology, applied in the field of solar cells, can solve problems such as corrosion, auxiliary electrode corrosion, and insulating layer corrosion, and achieve the effects of strong corrosion resistance, improved adhesion, and increased yield

Inactive Publication Date: 2013-01-02
IRICO
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0003] At present, the commonly used auxiliary electrode materials with high conductivity set on the conductive substrate are easily corroded by the electrolyte. Even if an inorganic insulating layer (commonly used dielectric material) is prepared on the auxiliary electrode, it can protect the electrode from electrolyte corrosion, but in titanium tetrachloride When the solution modifies the titanium dioxide film layer, the insulating layer protecting the auxiliary electrode is easily corroded by the titanium tetrachloride solution, resulting in the corrosion of the auxiliary electrode.

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  • Method for preparing dye-sensitized solar cell

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] A preparation method of a dye-sensitized solar cell, the specific preparation method of the cell comprises the following steps:

[0024] Preparation work: punch the conductive glass substrate 6 of the counter electrode according to the position of the graphic design, and then wash the conductive glass substrate 1 of the photoanode and the conductive glass substrate 6 of the counter electrode with detergent, acetone, ethanol, and deionized water in sequence. Ultrasonic cleaning, each cleaning time is 5-20 minutes, after cleaning, dry it with an air gun for later use. The conductive glass substrates 1 and 6 are conductive glass substrates of indium-doped tin oxide or fluorine-doped tin oxide.

[0025] Step 1: On the conductive glass substrate 1 of the photoanode and the conductive glass substrate 6 of the counter electrode, respectively print a layer of silver grid electrodes 3 and 8 by screen printing according to the designed pattern. Then dry it in an oven at 150°C fo...

Embodiment 2

[0035] A preparation method of a dye-sensitized solar cell, the specific preparation method of the cell comprises the following steps:

[0036] Preparations: the same preparations as in Example 1, and will not be repeated here.

[0037] Step 1: On the conductive glass substrate 1 of the photoanode and the conductive glass substrate 6 of the counter electrode, respectively print a layer of silver grid electrodes 3 and 8 by screen printing according to the designed pattern. Then dry it in an oven at 150°C for 20 minutes, and then transfer it to a resistance furnace for sintering at 500°C for 15 minutes. After the furnace temperature is lowered to room temperature, the conductive glass substrate 1 of the photoanode and the conductive glass substrate 6 of the counter electrode are taken out.

[0038] Step 2: Put the conductive glass substrate 1 of the photoanode into the electron beam evaporation chamber, and evaporate a layer of transparent LaB on the silver grid electrode accor...

Embodiment 3

[0047] A preparation method of a dye-sensitized solar cell, the specific preparation method of the cell comprises the following steps:

[0048] Preparations: the same preparations as in Example 1, and will not be repeated here.

[0049] Step 1: On the conductive glass substrate 1 of the photoanode and the conductive glass substrate 6 of the counter electrode, respectively print a layer of silver grid electrodes 3 and 8 by screen printing according to the designed pattern. Then dry it in an oven at 150°C for 20 minutes, and then transfer it to a resistance furnace for sintering at 490°C for 20 minutes. After the furnace temperature is lowered to room temperature, the conductive glass substrate 1 of the photoanode and the conductive glass substrate 6 of the counter electrode are taken out.

[0050] Step 2: Put the conductive glass substrate 1 of the photoanode into the electron beam evaporation chamber, and evaporate a layer of transparent LaB on the silver grid electrode accor...

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Abstract

The invention provides a method for preparing a dye-sensitized solar cell. The method comprises the following steps of: preparing a photo-anode conductive glass substrate printed with a silver gate electrode and a counter electrode conductive glass substrate; evaporating a transparent LaB6 layer on the silver gate electrode of the photo-anode conductive glass substrate; spraying a silane couplingagent layer on the photo-anode conductive glass substrate again; drying the silane coupling agent layer and printing a titanium dioxide thin film layer in a gap of the photo-anode silver gate electrode; sintering the photo-anode conductive glass substrate; placing the sintered photo-anode conductive glass substrate in prepared dye solution to dye-sensitize the titanium dioxide thin film layer to prepare a photo-anode; preparing an inorganic insulating layer on the counter electrode conductive glass substrate, printing a platinum electrode, and sintering the substrate to prepare a counter electrode; and finally butting the photo-anode and the counter electrode, pouring electrolyte and packaging. The method of the invention can protect the silver gate electrode from being corroded by solution of titanium tetrachloride and solution of electrolyte, so that the stability of a cell module is ensured.

Description

technical field [0001] The invention belongs to the technical field of solar cells, in particular to a preparation method of a dye-sensitized solar cell. Background technique [0002] Dye-sensitized solar cells are likely to become the leading solar cells in the future due to their simple manufacturing process and relatively low price. [0003] At present, the commonly used auxiliary electrode materials with high conductivity set on the conductive substrate are easily corroded by the electrolyte. Even if an inorganic insulating layer (commonly used dielectric material) is prepared on the auxiliary electrode, it can protect the electrode from electrolyte corrosion, but in titanium tetrachloride When the solution modifies the titanium dioxide thin film layer, the insulating layer protecting the auxiliary electrode is easily corroded by the titanium tetrachloride solution, thereby causing the auxiliary electrode to be corroded. Contents of the invention [0004] The purpose ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): H01L31/18H01L51/48H01G9/04H01G9/20H01M14/00
CPCY02E10/542Y02E10/50Y02E10/549Y02P70/50
Inventor 王香
Owner IRICO
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