Water-based tackifier resin emulsion and preparation method thereof
A tackifying resin emulsion, water-based technology, used in adhesives, rosin adhesives, etc., can solve problems such as harm to human health, poor adhesion and dispersibility, and achieve the effect of no harm to the human body and good adhesion
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[0024] Example 1
[0025] 1) Add 35.5 parts by mass of rosin glyceride, 42 parts by mass of rosin diethylene glycol ester, and 5 parts by mass of liquid terpene resin into the pre-emulsification kettle, blow in nitrogen, heat to 130-180°C to melt the resin, and then cool to 120-150°C, adjust the pH to 6-8 while stirring, then add 1 part by mass of nonylphenol polyoxyethylene ether amine sulfate and 1 part by mass of alkylphenol polyoxyethylene ether, and stir for 1 hour to form an emulsified resin liquid;
[0026] 2) Add 30 parts by mass of water and 15 parts by mass of pure acrylate polymer emulsion to the emulsification kettle, and heat to 85-100°C to form an aqueous solution of dispersant;
[0027] 3) Add the emulsion in 1) to the emulsification kettle in 2) while stirring, and turn on the emulsifier in the emulsification kettle to fully homogenize and disperse;
[0028] 4) Cool to below 40°C, adjust the pH to 6-8, then add 1.5 parts by mass of bactericide isoxazolinone, and then a...
Example Embodiment
[0030] Example 2
[0031] 1) Add 43.9 parts by mass of rosin pentaerythritol ester, 40 parts by mass of rosin methyl ester, and 10 parts by mass of liquid terpene resin into the pre-emulsification kettle, and then pass in nitrogen to replace the oxygen in the kettle, and heat to 130-180°C to melt the resin , Then lower the temperature to 120-150°C, adjust the pH to 6-8 while stirring, then add 3.1 parts by mass of rosin-based emulsifier, and keep stirring for 1.5 hours to form an emulsified resin liquid;
[0032] 2) Add 30 parts by mass of water and 8 parts by mass of pure acrylate polymer emulsion to the emulsification kettle, and heat to 85-100°C to form an aqueous solution of dispersant;
[0033] 3) Add the emulsion in 1) to the emulsification kettle in 2) while stirring, and turn on the emulsifier in the emulsification kettle to fully homogenize and disperse;
[0034] 4) Cool to below 40°C, adjust the pH to 6-8, add 0.18 parts by mass of the bactericide ninhydrin, and then add 19 ...
Example Embodiment
[0036] Example 3
[0037] 1) Add 19.5 parts by mass of rosin phenolic resin, 15 parts by mass of rosin triethylene glycol ester, and 35 parts by mass of liquid terpene resin into the pre-emulsification kettle, pass nitrogen into it, heat to 130-180°C to melt the resin, and then cool to 120-150℃, adjust the pH to 6-8 while stirring, then add 1.5 parts by mass of alkylphenol polyoxyethylene ether succinate sodium salt and 1 part by mass of nonylphenol polyoxyethylene ether, heat preservation and stir for 1.5 hours to form Emulsified resin liquid;
[0038] 2) Add 27 parts by mass of water and 5 parts by mass of vinyl acetate acrylate copolymer emulsion to the emulsification kettle, and heat to 85-100°C to form an aqueous solution of the dispersant;
[0039] 3) Add the emulsion in 1) to the emulsification kettle in 2) while stirring, and turn on the emulsifier in the emulsification kettle to fully homogenize and disperse;
[0040] 4) Cool to below 40°C, adjust the pH to 6-8, then add 0.1...
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