Adhesive composition, polarizing plate, and liquid crystal display
A composition, pressure-sensitive adhesive technology, applied in the direction of adhesive types, ester copolymer adhesives, adhesives, etc., can solve delayed resin and cross-linking agent reaction, large pressure-sensitive adhesive strength accumulation, decrease Removability and other issues to achieve the effect of suppressing light leakage, excellent workability and durability
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[0067]In the preparation of polarizers, the curing method of the pressure-sensitive adhesive composition according to the present invention is not particularly limited, for example, suitable heat or radiation capable of causing photoinitiation can be used to activate the thermal initiator contained in the composition. UV or electron beams activated by an agent are used for curing. In the present invention, the pressure-sensitive adhesive layer can be formed by using heat curing and radiation curing simultaneously.
[0068] In the present invention, if ray irradiation such as ultraviolet rays is used, ultraviolet irradiation can be performed by using, for example, a high-pressure mercury lamp, an induction lamp, or a xenon lamp. The radiation dose in ultraviolet curing is not particularly limited as long as it does not substantially impair physical properties and can sufficiently complete curing. For example, preferably its illumination intensity is 50-1,000mW / cm 2 and a radi...
Embodiment 1
[0080] Preparation of Acrylic Copolymer
[0081] 99 parts by weight of n-butyl acrylate (n-BA) and 0.1 part by weight of hydroxybutyl acrylate (HBA) were added to a 1 L reactor under nitrogen reflux and equipped with a cooling system for easy temperature control. Next, 120 parts by weight of ethyl acetate (EAc) was added as a solvent, and purged with nitrogen for 60 minutes to remove oxygen. Then the reactor was kept at 60°C, and 0.03 parts by weight of azobisisobutyronitrile (AIBN) was added as a reaction initiator, followed by a reaction for 8 hours, thereby preparing w / M n Acrylic resin for 3.4.
[0082] Preparation of pressure sensitive adhesive composition
[0083] With respect to 100 parts by weight of the prepared acrylic resin, by mixing 15 parts by weight of tris(acryloyloxyethyl) isocyanate (molecular weight: 423, trifunctional group, aronix M-315), 1.5 parts by weight as a photopolymerization initiator 1-hydroxycyclohexyl phenyl ketone, 1.5 parts by weight ...
Embodiment 2
[0089] A pressure-sensitive adhesive composition was prepared in the same manner as in Example 1, except that 1.5 parts by weight of 1,6-hexanediol was added instead of 1,4-butanediol as a pressure-sensitive adhesive strength stabilizer.
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