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Efficient anti-pollution isolation liquid for well cementation and preparation method thereof

An isolation fluid and anti-pollution technology, applied in chemical instruments and methods, drilling compositions, etc., can solve the problems of poor cement ring cementation quality and low displacement efficiency of two-phase fluid, avoid annular air channeling, and improve displacement. Efficiency, good chemical compatibility

Active Publication Date: 2012-10-31
SOUTHWEST PETROLEUM UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0011] The purpose of the present invention is to provide a high-efficiency anti-pollution spacer fluid for cementing to solve the problems of low efficiency of two-phase fluid contact pollution replacement and poor cement sheath cementation quality in cementing operations. 3 -2.60g / cm 3 The performance is controllable within the range, and the performance is stable in the temperature range of 40°C to 140°C; it has excellent anti-pollution performance, dilutes the drilling fluid and effectively isolates the drilling fluid and cement slurry, prevents contact pollution, and improves the displacement efficiency; Effective abrasion, scraping and displacement of attachments such as mud cake, dry dehydrated gelled and thickened drilling fluid, and improved cementing quality

Method used

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  • Efficient anti-pollution isolation liquid for well cementation and preparation method thereof
  • Efficient anti-pollution isolation liquid for well cementation and preparation method thereof
  • Efficient anti-pollution isolation liquid for well cementation and preparation method thereof

Examples

Experimental program
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Effect test

Embodiment 1

[0047] Wet preparation process: put 100 parts of water in the pulp cup, put 8 parts of sodium bentonite, stir for 3 hours; then put in 0.65 parts of sodium humate, 0.6 parts of hydroxyethyl cellulose, 0.5 parts of sodium sulfomethyl gallate , 0.1 part of sodium carbonate, stir well and adjust the performance to meet the requirements, put in 80 parts of barite powder to the required density; finally add 15 parts of sodium hydroxide to adjust the liquid pH between 8-11, and finally add 0.1 part of tributyl phosphate Stir for 1 hour to get density 1.3g / cm 3 High-efficiency anti-pollution isolation fluid for cementing.

Embodiment 2

[0049] Wet preparation process: put 100 parts of water in the pulp cup, put in 15 parts of polyethylene glycol, stir for 3 hours; then put in 3 parts of sodium sulfomethyl humate, 1 part of sodium carboxymethyl cellulose, 2 parts of iron Sodium chromium lignosulfonate, 5 parts calcium carbonate, stir evenly and adjust the performance to meet the requirements, put in 30 parts of ilmenite powder to the required density; finally add 10 parts of potassium hydroxide to adjust the pH of the spacer between 8-11, Finally, add 0.3 part of phenylethanol oleate and stir for 1 hour to obtain a density of 1.8g / cm 3 High-efficiency anti-pollution isolation fluid for cementing.

Embodiment 3

[0051] Dry preparation process: dry mix 28 parts of hydroxypropyl starch ether, 4 parts of sulfomethyl phenolic resin, 2 parts of sepiolite, 0.5 part of sodium carbonate, and 240 parts of magnetite powder into a mixed powder according to the weight ratio; Add 5 parts of sodium sulfomethyl digallate, 12 parts of sodium bicarbonate, and 0.2 parts of lauryl phenylacetate into 100 parts of clean water to prepare the base liquid of the isolation liquid and stir evenly; finally add the mixed powder to the base liquid of the isolation liquid ,Stir for 2 hours to get density 2.1g / cm 3 High-efficiency anti-pollution isolation fluid for cementing.

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Abstract

The invention relates to an efficient anti-pollution isolation liquid for well cementation and a preparation method thereof, belonging to the technical field of well cementation. The isolation liquid comprises the following components in parts by weight: 100 parts of clear water, 4-29 parts of suspending stabilizer, 0.5-5 parts of fluid loss additive, 0.3-2 parts of tackifier, 0.1-5 parts of diluting agent, 0-5 parts of viscosity and shearing force increasing agent, 30-350 parts of weighting agent, 1-25 parts of pH value regulating agent and 0.1-0.5 part of defoamer. The isolation liquid provided by the invention has wide density regulation range, large temperature resisting range, strong anti-pollution capacity, wide applicability and strong maneuverability, can be conveniently subjectedto in-situ preparation, can be prepared by using a mud tank equipment base fluid method or cement vehicle equipment dry-mixing method, and can apply effective abrasion, scraping and carrying effects to attachments on an interface of a well wall; and by using the isolation liquid, the problems that in the well cementation operation, pollution is generated by fluid displacement, the adhering quality of a well cementation interface is poor and the like are effectively solved.

Description

Technical field [0001] The invention relates to a high-efficiency anti-pollution isolation fluid for cementing and a preparation method thereof, which is used in the technical field of oil cementing engineering prefluid. Background technique [0002] The ultimate goal of cementing engineering is to ensure the quality of cementing, ensure that the cement ring is effectively sealed and cemented with the casing and the stratum, and prevent the oil, gas and water between different stratums from passing through each other, so as to ensure the normal exploitation and long-term exploitation of oil and gas wells. Later acidification fracturing to increase production is convenient. [0003] When cementing, use cement slurry to displace the drilling fluid, and form a cement ring in the annulus to support the casing and seal the formation. In this process, the complicated situations are as follows: [0004] (1) Contact pollution of drilling fluid and cement slurry [0005] The drilling fluid sy...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09K8/40
Inventor 郭小阳李早元程小伟刘洋马勇杨香艳李云杰焦少卿刘建李明
Owner SOUTHWEST PETROLEUM UNIV
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