Pyridaben microcapsule suspending agent and preparation method thereof

The technology of a microcapsule suspension and pyridaben, which is applied in the field of pesticides, can solve the problems that the pyridaben microcapsule suspension has not been effectively used, has not fully exerted its efficacy, and is harmful to human health, so as to prolong the effective period of the drug, Consolidate the effect of prevention and control, and the effect of less investment in equipment

Inactive Publication Date: 2012-08-08
GUANGDONG ZHONGXUN AGRI TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Pyridaben is now mainly focused on the research of emulsifiable oil, microemulsion, powder and wettable powder, and these formulations are easily damaged by the atmosphere, sunlight and rain, and the drug effect is not fully exerted, and they also kill natural enemies when killing pests. Destroy the ecological environment, pollute the environment, and more seriously, endanger human health due to residues in crops
[0004] At present, the main dosage forms of pyridaben acaricide products used in the pesticide market are emulsifiable concentrate and wettable powder, but the high-efficiency, low-toxicity, and environment-friendly pyridaben microcapsule suspension has not been effectively used

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] Example 1: 5% pyridaben microcapsule suspension.

[0024] Dissolve urea in formaldehyde, the weight ratio of urea and formaldehyde is 1:2, adjust the pH value to 8.5 with 10% sodium hydroxide aqueous solution, stir at a low speed at 70°C, and keep warm for 1 hour to obtain clear and transparent urea - Aqueous solution of formaldehyde resin prepolymer.

[0025] Dissolve 5% pyridaben in 15% xylene, add 2% Nongru 1601# to fully emulsify, stir at 30°C at a speed of 1000 rpm to fully disperse it, and obtain pyridaben mixture solution.

[0026] Add the urea-formaldehyde resin prepolymer aqueous solution to the pyridaben mixture solution stirred at 1000 rpm, stir for 15 minutes to form a stable emulsion, then reduce the stirring rate to 500 rpm, and slowly add an appropriate amount of Acetic acid, adjust its pH value to 5, and the temperature rises to 60°C to solidify the capsule wall. After 2 hours of reaction, the capsule wall is solidified. Use 10% sodium hydroxide aqueo...

Embodiment 2

[0027] Example 2: 10% pyridaben microcapsule suspension.

[0028] Dissolve urea in formaldehyde, the weight ratio of urea and formaldehyde is 1:2.5, adjust the pH value to 8.5 with 10% sodium hydroxide aqueous solution, stir at a low speed at 70°C, and keep warm for 1 hour to obtain clear and transparent urea - Aqueous solution of formaldehyde resin prepolymer.

[0029] Dissolve 10% pyridaben in 18% xylene, add 7% Nongru 700# to fully emulsify, stir at 30°C at a speed of 1000 rpm to fully disperse it, and obtain pyridaben mixture solution.

[0030] Add the urea-formaldehyde resin prepolymer aqueous solution to the pyridaben mixture solution stirred at 1000 rpm, stir for 15 minutes to form a stable emulsion, then reduce the stirring rate to 500 rpm, and slowly add an appropriate amount of Acetic acid, adjust its pH value to 5, and the temperature rises to 60°C to solidify the capsule wall. After 2 hours of reaction, the capsule wall is solidified. Use 10% sodium hydroxide a...

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Abstract

The invention discloses a pyridaben microcapsule suspending agent and a preparation method thereof. The pyridaben microcapsule suspending agent comprises: by weight, 1 to 10% of pyridaben, 3 to 20% of one or more capsule-core solvents, 5 to 30% of a capsule-wall material, 2 to 10% of one or more emulsifiers, 1 to 5% of one or more dispersants, 0.1 to 5% of one or more anti-freezing agents, 0.1 to 10% of a pH conditioning agent and the balance deionized water. The invention also discloses a preparation method of the pyridaben microcapsule suspending agent. The pyridaben microcapsule suspending agent has good physical chemistry stability and strong emulsification dispersibility and is a high-efficiency, wide-spectrum, low-toxicity and nuisance-free acaricide. The pyridaben microcapsule suspending agent solves the problem that pesticide effects can be influenced by the combination of pyridaben and soil, reduces a use amount through slow release thereby prolonging a pesticide validity period and consolidating control effects, inhibits that pesticides are decomposed by air, sunlight and rainwater and are lost, effectively controls the pollution on underground water and controls the change of the ecological environment.

Description

technical field [0001] The invention belongs to the field of pesticides, and in particular relates to a pyridaben microcapsule suspension and a preparation method thereof. Background technique [0002] Pyridaben, the Chinese name is Sufenling; High-efficiency, broad-spectrum acaricide, non-systemic, has obvious control effects on phytophagous harmful mites such as spider mites, panonychia, clawed mites and lean mites, and is effective against eggs, nymphs, and adults , It is also effective for the mobile period of adult mites. It is suitable for citrus, apple, pear, mountain ballast, cotton, tobacco, vegetables (except eggplant) and ornamental plants. Pyridaben is stable at 50°C for 90 days, stable in organic solvents, and unstable to light. [0003] Traditional types of pesticides such as EC, microemulsion, powder and wettable powder account for more than 90% of the total preparations in my country. With the development of processed dosage forms, the disadvantages of tra...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A01N43/58A01N25/28A01N25/04A01P7/02
Inventor 曹希敏孟宪秋王龙江刘华金袁彩斌
Owner GUANGDONG ZHONGXUN AGRI TECH
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