Method for preparing compound powder of alumina and chrome oxide from chromium-containing aluminum sludge
A composite powder, chromium oxide technology, applied in the direction of improving process efficiency, can solve problems such as pollution, and achieve the effects of no by-products, eradication of pollution problems, and control of product components
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[0027] Example 1:
[0028] Weigh 30 g of chromium-aluminum mud into a beaker, add 180 mL of 3 mol / L hydrochloric acid, heat to 80 ℃ under stirring, continue stirring, and keep it warm until all chromium-aluminum mud is dissolved to obtain an aluminum mud solution. Determine the concentration of Cr(Ⅲ), Cr(Ⅵ) and Al(Ⅲ) in the aluminum sludge dissolved solution and convert them to Cr 2 O 3 , Cr 2 O 3 , Al 2 O 3 The mass ratio is 1:1.5:100, adding 1 g of glucose, stirring, after the reaction is complete, standing, and cooling to room temperature. Add NaOH solution to pH 3.5, filter to remove Si and Fe impurities. Add 2.5 mL polyethylene glycol 400, mix well, add NaOH solution to pH 7.7 to obtain Al(OH) 3 , Cr(OH) 3 Mix the precipitate and obtain the filtrate and filter cake after filtration. The filter cake is washed with water until the washing liquid does not contain Cr (VI), and the washing liquid is combined into the filtrate. The filter cake was air-dried at 120 ℃ until the p...
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[0029] Example 2:
[0030] Weigh 50 g of chromium-aluminum mud in a beaker, add 50 mL of 6 mol / L sulfuric acid, heat to 100 ℃ under stirring, continue stirring, and keep it warm until all chromium-aluminum mud is dissolved to obtain an aluminum mud solution. Determine the concentration of Cr(Ⅲ), Cr(Ⅵ) and Al(Ⅲ) in the aluminum sludge dissolved solution and convert them to Cr 2 O 3 , Cr 2 O 3 , Al 2 O 3 Calculate, the mass ratio is 2:1:100, add 2 g of sucrose, stir, after the reaction is complete, stand still and cool to 50°C. Add NaOH solution to pH 3.0, filter to remove Si and Fe impurities. Add 5 mL of absolute ethanol, mix well, add NaOH solution to pH 7 to obtain Al(OH) 3 , Cr(OH) 3 Mix the precipitate and obtain the filtrate and filter cake after filtration. The filter cake is washed with water until the washing liquid does not contain Cr (VI), and the washing liquid is combined into the filtrate. The filter cake was air-dried at 100 ℃ until the powder became dry and easi...
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[0031] Example 3:
[0032] Weigh 30 g of chromium-containing aluminum mud into a beaker, add 150 mL of 5 mol / L nitric acid, heat to 30 ℃ under stirring, continue stirring, and keep the temperature until all the chromium-containing aluminum mud is dissolved to obtain an aluminum mud solution. Determine the concentration of Cr(Ⅲ), Cr(Ⅵ) and Al(Ⅲ) in the aluminum sludge dissolved solution and convert them to Cr 2 O 3 , Cr 2 O 3 , Al 2 O 3 Calculate, the mass ratio is 2:3:100, add 1 mL of formaldehyde, stir, after the reaction is complete, stand still and cool to room temperature. Add NaOH solution to pH 2.5, filter to remove Si and Fe impurities. Add 5g of sodium dodecyl sulfonate with the mass of the solution, mix well, add NaOH solution to pH 6.8 to obtain Al(OH) 3 , Cr(OH) 3 Mix precipitation. Add 0.3 mL of 5‰ polyacrylamide flocculant, filter after precipitation is complete, and obtain filtrate and filter cake. The filter cake is washed with water until the washing liquid doe...
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