Gas separation membrane for dme production process
A technology of gas separation membrane and production process, which is applied in the fields of hydrogen separation, gas treatment, separation methods, etc.
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Embodiment 1
[0060] (a) Preparation of hollow fiber membrane
[0061] 20g polyetherimide (Sabic-IP company, Ultem TM ), 20 g of tetrahydrofuran (first additive) and 20 g of ethanol (second additive) were sequentially and slowly added dropwise to 40 g of N-methylpyrrolidone (solvent) while stirring the solvent, thus preparing a uniform spinning solution. Subsequently, air bubbles were removed from the spinning solution at room temperature and reduced pressure for 24 hours, and then foreign materials were removed from the spinning solution with a 60 μm filter. Subsequently, the spinning solution was spun at a temperature of 60° C. with a cylinder pump at a flow rate of 7 cc / min. Here, the air gap was 10 cm, a double spinneret was used, and water was used as a coagulant. Further, the inner diameter and the outer diameter of the inner nozzle of the double spinning head were 0.4 mm and 0.8 mm, respectively, and the diameter of the outer nozzle of the double spinning head was 1.2 mm. Subseque...
Embodiment 2
[0069] The hollow fiber membrane prepared in the same manner as in Example 1 was unwound from the bobbin, and then immersed in a 5% polyethylene oxide-urethane coating solution (solvent: n-butane) at room temperature for 5 seconds or longer , while maintaining a constant tension to fabricate a gas separation membrane comprising a composite membrane coated with a separation material. A gas separation membrane module was manufactured using the manufactured gas separation membrane, and then the performance of the gas separation membrane module was evaluated in the same manner as in Example 1. The results are given in Table 2 below.
[0070] 【Table 2】
[0071]
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