Preparation method of black-bone chicken peptide and iron chelated biological iron supplement
The technology of chelate and black chicken peptide is applied in the field of preparation of black chicken peptide iron chelate biological iron supplement, which can solve the problems of low absorption and utilization rate, oxidative damage, unclear molecular weight of components, etc. Fast absorption, good effect of iron supplementation
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Embodiment 1
[0039] Preparation of the black-bone peptide solution: Weigh 10.0 g of the black-bone peptide and place it in a reaction vessel, add 250 mL of distilled water, stir and dissolve to obtain a black-bone peptide solution with a concentration of 4%.
[0040] Chelate ferrous ion: Weigh 2.5g of ascorbic acid, dissolve it in the black-bone peptide solution to make the concentration reach 1.0%, prevent the oxidation of ferrous ion, add 10g of ferrous chloride, make the black-bone peptide and ferrous chloride in the mixed solution The mass ratio is 1:1. Stir to fully dissolve the reaction, adjust and maintain the pH value of the solution at 5, place the liquid in a reaction tank at 30°C for 40 minutes, and keep the reaction in a closed environment to avoid oxidation of ferrous ions.
[0041] Concentration: the reaction solution was left to cool, placed in a vacuum concentration device, and the volume of the reaction solution was reduced at 45° C. using the vacuum concentration device. ...
Embodiment 2
[0045] Preparation of the black-bone peptide solution: Weigh 5 kg of the black-bone peptide and place it in a reaction tank, add 100 L of distilled water, stir and dissolve to prepare a 5% black-bone peptide solution.
[0046] Chelate ferrous ions: Weigh 0.8kg of ascorbic acid, dissolve it in the black-bone peptide solution to make the concentration reach 0.8%, prevent the oxidation of ferrous ions, weigh 2.5kg of ferrous sulfate and add it to the mixed solution, so that the black-bone peptide in the mixed solution The mass ratio of ferrous sulfate to ferrous sulfate is 2:1, stir to dissolve it. Adjust the pH value to keep it at about 6, stir to make it fully react at 40°C for 30min. Keep a closed environment during the reaction to prevent ferrous ions from contacting air oxidation.
[0047] Concentration: The reaction solution was left to cool, then transferred to a vacuum concentration device, and the volume of the reaction solution was reduced at 50°C by using the vacuum c...
Embodiment 3
[0052] Preparation of black-bone peptide solution: Weigh 3.0 kg of black-bone peptide and place it in a reaction vessel, add 100 L of distilled water, stir and dissolve to obtain a black-bone peptide solution with a concentration of 3%.
[0053] Chelated ferrous ion: Weigh 1.2kg of ascorbic acid, dissolve it in the black-bone peptide solution to make the concentration reach 1.2%, prevent the oxidation of ferrous ion, add 1.0kg ferrous chloride, make the black-bone peptide and ferrous chloride in the mixed solution The mass ratio of iron is 3:1. Stir to fully dissolve the reaction, adjust and maintain the pH value of the solution at 3, place the liquid in a reaction tank at 60°C for 20 minutes, and keep the reaction in a closed environment to avoid oxidation of ferrous ions.
[0054] Precipitation and drying: add absolute ethanol to the chelating solution at a volume ratio of 1:3, the unit is L / L, place it at room temperature for precipitation for 2 hours, wash with absolute et...
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