Application and preparation of high-activity composite oxide oxygen carrier in chemical link circulation hydrogen production
An oxygen carrier and oxide technology, applied in the field of chemical chain hydrogen production, can solve the problems of low dispersity of metal oxides, low cyclic reactivity, limited oxygen carrying rate, etc. Simple method and low cost effect
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Embodiment 1
[0019] Take 21.85gCo(NO 3 ) 2 ·6H 2 Put O into a 500mL beaker, add 100mL of distilled water, slowly dropwise add chloropalladium acid solution containing 4% Pd, and then add 100mL of distilled water to make the molar ratio of Co to Pd 0.95 / 0.05, then place the beaker at 80 In a water bath at ℃, the stirring speed is 400rpm, and stir until completely dissolved. Take 30.87g La(NO 3 ) 3 ·6H 2 O and 0.8g KNO 3 Put it into a beaker with 100mL of distilled water and stir until it is completely dissolved so that the molar ratio of La to K is 0.9 / 0.1. Then add the lanthanum nitrate and potassium nitrate solution dropwise to the cobalt nitrate and chloropalladium acid solution, and stir while adding dropwise. Take 40g of citric acid, the molar ratio of citric acid to the total amount of metal ions is 1.2:1, put it into a 100mL beaker and stir until it is completely dissolved. At this time, after the above mixed solution is stirred for 30 minutes, slowly add the citric acid solut...
Embodiment 2
[0021] Take 20.7gCo(NO 3 ) 2 ·6H 2 Put O into a 500mL beaker, slowly add 4% Pd-containing chloropalladium acid solution dropwise, then add 100mL of distilled water to make the molar ratio of Co to Pd 0.9 / 0.1, then place the beaker in a water bath at 80°C, Stirring speed is 400rpm, stir until completely dissolved. Take 29.15g La(NO 3 ) 3 ·6H 2 O and 1.2g KNO 3Put it into a beaker with 100mL of distilled water, stir until it is completely dissolved, so that the molar ratio of La to K is 0.85 / 0.15. Then add the lanthanum nitrate and potassium nitrate solution dropwise to the cobalt nitrate and chloropalladium acid solution, and stir while adding dropwise. Take 67g of citric acid, the molar ratio of citric acid to metal ions is 1.2:1, put it into a 100mL beaker and stir until it is completely dissolved. After the above mixed solution is stirred for 30 minutes, slowly add the citric acid solution, while adding While stirring. After stirring for 5 hours, the brown solution ...
Embodiment 3
[0023] Take 21.85gCo(NO 3 ) 2 ·6H 2 Put O into a 500mL beaker, add 100mL of distilled water, slowly dropwise add chloropalladium acid solution containing 4% Pd, and then add 100mL of distilled water to make the molar ratio of Co to Pd 0.95 / 0.05, then place the beaker at 80 In a water bath at ℃, the stirring speed is 400rpm, and stir until completely dissolved. Take 27.44g La(NO 3 ) 3 ·6H 2 O and 1.6g KNO 3 Put it into a beaker with 100mL of distilled water and stir until it is completely dissolved so that the molar ratio of La to K is 0.8 / 0.2. Then add the lanthanum nitrate and potassium nitrate solution dropwise to the cobalt nitrate and chloropalladium acid solution, and stir while adding dropwise. Take 40g of citric acid, the molar ratio of citric acid to the total amount of metal ions is 1.2:1, put it into a 100mL beaker and stir until it is completely dissolved. After the above mixed solution is stirred for 30 minutes, slowly add the citric acid solution, while add...
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