Method for preparing modified amino acid chelated iron feed additive
A feed additive and amino acid technology, applied in animal feed, animal feed, applications, etc., can solve the problems of low amino acid concentration, low product chelation rate, long reaction cycle, etc., and achieve small amino acid molecular weight, low chelation rate, and reaction short cycle effect
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[0021] 1. Preparation of modified amino acid chelated iron
[0022] In the reaction vessel, add 1200ml of 20% sulfuric acid, then add 1000g of feather meal, and perform hydrolysis reaction at 100-105°C for 70min to completely dissolve the feather meal. After cooling, add 200g of ferrous sulfate, then add sodium hydroxide solution, adjust the pH value to 6.0, and react at 100-105°C for 6 hours; after the reaction, cool to 45°C, add an appropriate amount of protease, and then react for 12 hours , to obtain amino acid iron chelate iron; then add 1000g acetic acid, 200g montmorillonite powder, 400g polyethylene glycol 4000, and 200g poplar bark powder to the reaction solution, and finally adopt three-effect concentration technology to concentrate and dry to obtain modified amino acid chelate Iron Feed Additive.
[0023] Detection method: The content of chelated iron was measured by o-phenanthroline colorimetric method.
[0024] 2. Feeding test
[0025] (1) Test material
[002...
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