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Light-weight Al2O3-SiC-C refractory casting material and preparation method thereof

An al2o3-sic-c, refractory castable technology, applied in the field of lightweight castables, can solve the problems of inability to directly use working layers, poor slag corrosion resistance, and inapplicability, and achieve controllable apparent porosity and medium resistance. The effect of strong erosion ability and controllable pore size

Inactive Publication Date: 2013-03-13
WUHAN UNIV OF SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, they have poor resistance to slag erosion and cannot be directly used in the working layer
The material described in "A Aluminum-Magnesium Lightweight Castable and Its Preparation Method (ZL200610125542.7)" has high resistance to alkaline slag erosion and good thermal insulation effect, but it is not suitable for acid slag as the main environment. High temperature molten iron storage and transportation equipment

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0034] A light Al 2 o 3 -SiC-C refractory castable and its preparation method: 15~18wt% of porous corundum particles with a particle size of 8~5mm, 15~20wt% of porous corundum particles with a particle size of 5~3mm, 10~12wt% of porous corundum particles Porous corundum particles with a diameter of 3~1mm, 9~12wt% white corundum particles, 9~12wt% SiC particles, 8~10wt% SiC fine powder, 6~8wt% corundum fine powder, 10~12wt% Activated alumina fine powder, 3~5wt% calcium aluminate cement, 2~4wt% silica fine powder, 2~4wt% spherical pitch, 1.5~2.0wt% silicon powder, 0.1~0.3wt% aluminum powder and 0.1~0.3wt% boron carbide powder is used as raw material, and then 10~15wt% water, 0.2~0.4wt% sodium tripolyphosphate and 0.02~0.04wt% organic explosion-proof fiber are added to the raw materials, stirred evenly, and casted ; The molded green body is naturally dried for 24 hours, and then dried at 110°C for 24 to 48 hours to obtain light Al 2 o 3 -SiC-C refractory castable.

[0035] I...

Embodiment 2

[0038] A light Al 2 o 3 -SiC-C refractory castable and its preparation method: 17~20wt% of porous corundum particles with a particle size of 8~5mm, 17~22wt% of porous corundum particles with a particle size of 5~3mm, 11~13wt% of porous corundum particles Porous corundum particles with a diameter of 3~1mm, 8~10wt% brown corundum particles, 6~10wt% SiC particles, 6~8wt% SiC fine powder, 5~7wt% corundum fine powder, 8~10wt% Activated alumina fine powder, 3~5wt% calcium aluminate cement, 2~4wt% silica fine powder, 2~4wt% spherical pitch, 1.5~2.0wt% silicon powder, 0.1~0.3wt% aluminum powder and 0.1-0.3wt% boron carbide powder is used as a raw material, plus 8-13wt% water, 0.2-0.4wt% sodium hexametaphosphate and 0.02-0.04wt% organic explosion-proof fiber, stirred evenly, and poured; The molded green body is naturally dried for 24 hours, and then dried at 110°C for 12 to 36 hours to obtain light Al 2 o 3 -SiC-C refractory castable.

[0039] In this embodiment: the apparent poro...

Embodiment 3

[0042] A light Al 2 o 3 -SiC-C refractory castable and its preparation method: 16~19wt% of porous corundum particles with a particle size of 8~5mm, 16~21wt% of porous corundum particles with a particle size of 5~3mm, 10~12wt% of porous corundum particles Porous corundum particles with a diameter of 3~1mm, 9~12wt% platy corundum particles, 8~10wt% SiC particles, 7~9wt% SiC fine powder, 6~8wt% corundum fine powder, 9~11wt% Activated alumina powder, 3~5wt% calcium aluminate cement, 2~4wt% silica powder, 2~4wt% spherical pitch, 1.5~2.0wt% silica powder, 0.1~0.3wt% aluminum powder And 0.1~0.3wt% boron carbide powder as raw material, add 9~14wt% water, 0.2~0.4wt% polycarboxylate water reducer and 0.02~0.04wt% organic explosion-proof fiber, and stir evenly , casting molding; the molded green body is naturally dried for 24 hours, and then dried at 110°C for 18 to 40 hours to obtain light Al 2 o 3 -SiC-C refractory castable.

[0043] In this embodiment: the apparent porosity of th...

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Abstract

The invention relates to a light-weight Al2O3-SiC-C refractory casting material and a preparation method thereof. The light-weight Al2O3-SiC-C refractory casting material comprises the following raw materials: 40-55 wt% of porous corundum particle, 8-12 wt% of corundum particle, 6-12 wt% of SiC particle, 6-10 wt% of SiC fine powder, 5-8 wt% of corundum fine powder, 8-12 wt% of active aluminum oxide micropowder, 3-5 wt% of calcium aluminate cement, 2-4 wt% of silicon oxide micropowder, 2-4 wt% of ball asphalt, 1.5-2.0 wt% of silicon powder, 0.1-0.3 wt% of aluminum powder and 0.1-0.3 wt% of boron carbide powder. The preparation method comprises the following steps: mixing the raw materials with 8-15 wt% of water, 0.2-0.6 wt% of water reducing agent and 0.02-0.04 wt% of organic explosion-proof fiber, stirring, casting, molding, and naturally drying at 110 DEG C for 12-48 hours to obtain the light-weight Al2O3-SiC-C refractory casting material. According to the invention, the process is simple; and the prepared product has the characteristics of high strength, excellent thermal shock stability, low heat conductivity and high medium erosion resistance, and also has the advantage that the apparent porosity and pore size can be controlled.

Description

technical field [0001] The invention belongs to the technical field of lightweight castables. Specifically related to a light Al 2 o 3 -SiC-C refractory castable and preparation method thereof. Background technique [0002] al 2 o 3 -SiC-C and Al 2 o 3 -SiC refractories are the main lining materials for special equipment for storage, transportation and processing of high-temperature molten iron, such as tapping troughs, torpedo-type mixed iron cars, mixed iron furnaces, and ladles (tanks). Refractory materials are composed of aggregate and matrix. Traditional Al 2 o 3 -SiC-C and Al 2 o 3 -SiC refractory materials are dense refractory materials, usually with dense white corundum, brown corundum and alumina as aggregates. In order to prepare dense aggregate, raw materials must be sintered or fused at high temperature, which will cause a lot of energy consumption and environmental pollution; at the same time, dense Al 2 o 3 -SiC-C and Al 2 o 3 -SiC refractories ...

Claims

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Application Information

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IPC IPC(8): C04B35/66C04B35/10C04B35/626
Inventor 鄢文李楠陈俊峰苗正魏耀武韩兵强柯昌明
Owner WUHAN UNIV OF SCI & TECH
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