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Equipment and process for producing high-performance polyphenylene sulfide fine-denier fiber

A technology for polyphenylene sulfide and fine denier fiber, which is applied in the process of producing polyphenylene sulfide fine denier fiber and the field of polyphenylene sulfide fine denier fiber production equipment, can solve the problem that technical indicators such as strength and elongation are difficult to meet requirements , It is difficult to produce polyphenylene sulfide fine denier fibers, equipment and process requirements are high, so as to reduce the amount of oxygen entering, reduce the residence time, and improve product quality.

Active Publication Date: 2013-04-03
SICHUAN UNFIRE POLYMER MATERIALS TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, domestic conventional varieties of polyphenylene sulfide fiber (above linear density 2.2dtex) can basically be self-sufficient, but polyphenylene sulfide fine denier fiber (linear density below 2.0dtex) can only rely on foreign imports, and domestic production is still not possible. The main reason is that The equipment and process requirements for the production of polyphenylene sulfide fine denier fibers are relatively high
[0004] At present, due to the performance limitations of the drying system, screw extruder, spinneret, cooling device and other components of the domestic production of polyphenylene sulfide fiber, it is difficult to produce polyphenylene sulfide fine denier fiber, or its strength, elongation, etc. Long rate and other technical indicators are difficult to meet the requirements

Method used

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  • Equipment and process for producing high-performance polyphenylene sulfide fine-denier fiber
  • Equipment and process for producing high-performance polyphenylene sulfide fine-denier fiber
  • Equipment and process for producing high-performance polyphenylene sulfide fine-denier fiber

Examples

Experimental program
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Effect test

Embodiment 1

[0027] Such as figure 1 , figure 2 and image 3 As shown, a kind of high-performance polyphenylene sulfide fine-denier fiber production equipment of the present invention comprises a drying system 1, a screw extruder 2, a filter 3, a spinning machine 4 and a cooling device 5 connected in sequence, and the drying system 1 includes a drier 6, the air outlet 7 and the air inlet 8 of the drier 6 are closed and connected in sequence through a gas delivery pipe to a gas purification processor 9, a gas dehumidification processor 10, a fan 11, and a heater 12. The drying The feed port of the machine 6 is connected with an intermediate feed bin 13, and the discharge port of the dryer 6 is connected with an intermediate feed bin 14, and the feed port of the intermediate feed bin 13 is provided with a valve 15 and a discharge port. There is valve two 16, the feed port of the intermediate silo two 14 is provided with valve three 17, and the discharge port is provided with valve four 18...

Embodiment 2

[0029]A kind of technology that adopts the equipment in embodiment 1 of the present invention to produce high-performance polyphenylene sulfide fine denier fiber, comprises the following steps: A, material selection: select melting finger to be in 150-250g / min, molecular weight distribution in ± 2% scope The raw materials inside are cleaned of impurities; B, drying: the raw materials after cleaning are sent to the drying system for crystallization and drying at 100-170°C for 3-16 hours, so that the water content is less than 50ppm; C, melting: reuse The screw extruder is heated to 290-350°C for melting; D, spinning: after the melt impurities are filtered out by a filter, it is sent to the spinning machine for spinning under the condition of 350°C heat preservation and 2MPa pressure; E, cooling : After passing through the circular heating and slow cooling channel at 120°C, the sprayed filaments enter the circular air blowing channel under the conditions of 30°C and relative humi...

Embodiment 3

[0031] A kind of technology that adopts the equipment in embodiment 1 of the present invention to produce high-performance polyphenylene sulfide fine denier fiber, comprises the following steps: A, material selection: select melting finger to be in 150-250g / min, molecular weight distribution in ± 2% scope The raw materials inside are cleaned of impurities; B, drying: the raw materials after cleaning are sent to the drying system for crystallization and drying at 100-170°C for 3-16 hours, so that the water content is less than 50ppm; C, melting: reuse The screw extruder is heated to 290-350°C for melting; D, spinning: after the melt impurities are filtered out by a filter, it is sent to the spinning machine for spinning under the condition of 290°C heat preservation and 15MPa pressure; E, cooling : After passing through the circular heating and slow cooling channel at 80°C, the sprayed filaments enter the circular blowing channel at 20°C and relative humidity of 90 for cooling, ...

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Abstract

The invention discloses equipment and a process for producing high-performance polyphenylene sulfide fine-denier fiber. The equipment comprises a drying system, a screw extruder, a filter, a spinning machine and a cooling device which are connected sequentially, wherein the drying system comprises a drying machine; a gas purification processor, a gas dehumidification processor, a fan and a heater are sequentially connected through gas delivery pipes in a sealed manner between a gas outlet and a gas inlet of the drying machine; the draw ratio of a screw rod of the screw extruder ranges from 26 to 32; the depth of a screw groove at the tail end of the metering section of the screw rod is 3 to 5 mm; an annular spinneret plate is mounted at the lower end of the spinning machine; and a plurality of concentric annular flow guide grooves and radial communicated flow guide grooves are formed in the annular spinneret plate. The process comprises the steps of selecting materials, drying, fusing, jetting silk, cooling and the like. According to the equipment and the process, the structures of a plurality of parts are improved; process steps and parameters are optimized; the produced polyphenylene sulfide fine-denier fiber has high quality stability; the qualified rate of products is high; and according to detection, the polyphenylene sulfide fine-denier fiber reaches or even exceeds the industrial standard and import products in multiple performance parameters.

Description

technical field [0001] The invention relates to a polyphenylene sulfide fiber production equipment, in particular to a polyphenylene sulfide fine-denier fiber production equipment, and also relates to a process for producing polyphenylene sulfide fine-denier fibers using the equipment. Background technique [0002] Polyphenylene sulfide fiber is a new type of special fiber, which is made of polyphenylene sulfide resin (PPS) by conventional melt spinning method, and then stretched, crimped and cut at high temperature. Its short fiber has excellent thermal stability and flame retardancy, its chemical resistance is second only to polytetrafluoroethylene fiber, and it has better textile processing performance. The products are mainly used for the filtration of high temperature flue gas and special heat medium, the drying belt of the paper industry, the cable covering layer and the fireproof fabric, etc. [0003] Polyphenylene sulfide fiber is an important variety in the develop...

Claims

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Application Information

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IPC IPC(8): D01D13/00D01D4/02D01D5/092D01D1/00D01D1/04
Inventor 李文俊李亚儒叶光斗刘鹏清甘为宋召碧赵发燕
Owner SICHUAN UNFIRE POLYMER MATERIALS TECH
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