Preparation method of titanium dioxide-graphene composite nano paper
A technology of graphene composite and titanium dioxide, which is applied in the direction of titanium dioxide, graphene, titanium oxide/hydroxide, etc., can solve the problems of application limitation and photocatalytic activity reduction, and achieve the goal of promoting application, simple production method and broad application prospect Effect
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Embodiment 1
[0031] A titanium dioxide-graphene composite nano paper, the main components of which are titanium dioxide nanobelts and graphene or titanium dioxide nanobelts, graphene and additives.
[0032] The preparation method of the above titanium dioxide-graphene composite nano paper. It mainly includes synthesis-composite-dispersion-suction filtration-drying and other processes. Concrete preparation process is as follows:
[0033] (1) Preparation of titanium dioxide nanoribbons
[0034] Weigh 0.5 ~ 1g titanium dioxide powder to place in 30 ~ 50 mL KOH (10 ~ 15 mol?L -1 ) solution in a polytetrafluoroethylene-lined stainless steel reactor, after ultrasonic treatment for 10 min, close and tighten the reactor, and react in a preheated oven at 170°C to 220°C for 20 to 60 hours. After the reaction was completed, it was naturally cooled to room temperature, and the product in the kettle was poured out, washed with ultrapure water until neutral to obtain potassium titanate nanobelts. ...
Embodiment 2
[0043] The preparation steps were the same as in Example 1, except that 1 g of titanium dioxide-graphene composite nanomaterial was weighed and placed in 1 L of water, and ultrasonically dispersed for 1 h to form a titanium dioxide-graphene suspension.
Embodiment 3
[0045] The preparation steps were the same as in Example 1, except that 0.1 g of titanium dioxide-graphene composite nanomaterial was weighed and placed in 1 L of water, and magnetically stirred and dispersed for 1 h to form a titanium dioxide-graphene suspension.
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