Method for degumming ramie

A technology of hemp degumming and volume fraction, applied in the field of hemp degumming, can solve the problems of large water consumption, complicated process, difficult to control, etc., and achieve the effect of simple and convenient degumming process, good degumming effect and reduced loss

Inactive Publication Date: 2013-08-28
WUHAN TEXTILE UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, its disadvantage is that the equipment used for ultrasonic degumming is relatively expensive, and the investment is large, and there is a certain amount of noise in the ultrasonic wave.
However, its disadvantage is that the process conditions of this method are complex and difficult to control.
However, its disadvantage is that this method requires special mechanical equipment, and the process is complicated.
However, its disadvantage is that the method needs to cultivate strains first, and the process is relatively complicated.
Although it adopts the method of microwave irradiating hemp degumming to prepare fibers, it does shorten the degumming process and improve the degumming efficiency, but its disadvantage is that this method will use a large amount of water in the degumming process, and there is no fundamental Solve the problem of large water consumption for degumming, and the waste water after degumming is difficult to recycle
Although the method of degumming ramie with a mixture of acid pectinase, acid cellulase and acid protease did improve degumming efficiency, reduce cost and energy consumption, but its disadvantage is that it may have enzyme Solve the problem of low efficiency
Although it uses organic solvents to degumming hemp, it does have a good degumming effect and an alkali-free and acid-free degumming process, but its disadvantages are that most of the organic solvents used in this method are toxic substances, and the organic solvents are only used for extracting wood. The raw material of element, and still adopt in this degumming method
Although the biological enzyme degumming method it adopts does play a role in simplifying the process steps, reducing costs and improving efficiency, its disadvantage is that this method does not fundamentally solve the problem of large water consumption, and biological enzyme degumming has certain limitations sex

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0041] According to the above process steps: 1g of ramie is selected for degumming, and the alcoholic organic solvent is selected as ethanol. Put ramie in an acid solution mixed with ethanol with a volume fraction of 95%, water with a volume fraction of 5%, and sulfuric acid with a concentration of 2g / L for pickling treatment. The acid bath ratio is 1:30, and the pickling temperature is The temperature is 60°C, and the pickling time is 60 minutes. The ramie after pickling treatment is placed in the lye mixed with 95% ethanol, 5% water and 6g / L sodium hydroxide for scouring treatment. The ratio is 1:30, the scouring temperature is 130°C, and the scouring time is 2 hours. Put the ramie after scouring with lye into the bleaching solution mixed with ethanol with a volume fraction of 95%, water with a volume fraction of 5%, and sodium hypochlorite with an available chlorine concentration of 1.5g / L for bleaching treatment. The bath ratio is 1:30, the pH is 11, the bleaching temper...

Embodiment 2

[0043] According to the above process steps: 1g of flax is selected for degumming, and the alcoholic organic solvent is selected as isopropanol. Put flax in an acid solution mixed with 50% isopropanol by volume, water with 50% volume and sulfuric acid with a concentration of 1g / L for pickling treatment. The acid bath ratio is 1:10. The acid temperature is 50°C, and the pickling time is 30 minutes. Put the flax after pickling treatment in the lye mixed with 50% isopropanol, 50% water and 5g / L sodium hydroxide for scouring treatment. The bath ratio is 1:10, the scouring temperature is 100°C, and the scouring time is 1 hour. The flax scoured by lye is placed in the bleaching solution mixed with 50% isopropanol by volume, water with 50% by volume, and sodium hypochlorite with an available chlorine concentration of 1g / L for bleaching treatment. The liquid bath ratio is 1:10, the pH is 9, the bleaching temperature is 20°C, and the bleaching time is 30 minutes. Put the bleached he...

Embodiment 3

[0045] According to the above process steps: select 1g of jute for degumming, and the alcoholic organic solvent is selected as ethanol. The jute is placed in the acid solution that the volume fraction is 70% alcohol ethanol, the volume fraction is 30% water, and the sulfuric acid that the concentration is 1.5g / L mixes and carries out pickling treatment, and the acid bath ratio is 1:20, The pickling temperature is 55°C, and the pickling time is 40 minutes. The jute after the pickling treatment is placed in the lye mixed with 70% ethanol, 30% water and 5.5g / L sodium hydroxide for scouring. The bath ratio is 1:20, the scouring temperature is 120°C, and the scouring time is 1.5 hours. The jute after lye scouring is placed in the bleaching solution that the volume fraction is 70% ethanol, the volume fraction is 30% water, and the sodium hypochlorite that the available chlorine concentration is 1.3g / L mixes and carries out bleaching treatment, bleaching solution The bath ratio is ...

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Abstract

The invention relates to a method for degumming ramie. The method adopts the solution formed by mixing a high-proportion alcohol organic solvent with a small amount of water and degumming reagent to carry out the degumming treatment on the ramie, thus effectively improving the solubility of impurities such as hemicellulose, pectin, cerolipoid and ash, and reducing the degumming difficulty of the ramie; and furthermore, the loss of the strength of ramie fiber is greatly reduced, so that the quality of the ramie fiber is improved, and the ramie fiber is high in quality and efficiency. The degumming technology is simple and convenient, good in degumming effect and high in efficiency, greatly reduces the water consumption in the degumming process of the ramie, and effectively reduces the dosage of a chemical reagent; and the alcohol organic solvent not only is safe and non-toxic, but also can be recycled, so that the method is low in pollution, low in cost, clean, energy-saving, safe and environment-friendly.

Description

technical field [0001] The invention relates to a method for degumming hemp. Specifically, the hemp is degummed by using a solution mixed with a high proportion of alcohol organic solvent, a small amount of water and a degumming reagent. Background technique [0002] my country is a big country in the world of hemp textiles, including ramie, flax, kenaf, jute, hemp and other hemp crops. The hemp fiber textile raw material has won people's favor as a clothing fabric because of its unique excellent performance. However, there have always been many problems in the textile processing technology of hemp, among which the degumming process has always restricted the processing quality of hemp products, and even affected the performance of hemp textiles. Therefore, degumming is a key link in the production of hemp textiles. [0003] The hemp bark directly peeled off from the hemp stalk is called raw hemp. In addition to the cellulose component, the raw hemp also contains a certain a...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D01C1/02
Inventor 徐卫林夏良君程珊王运利
Owner WUHAN TEXTILE UNIV
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