Composite nanocapsule phase-change material and preparation method thereof
A technology of nanocapsules and phase change materials, applied in heat exchange materials, chemical instruments and methods, silicon oxide, etc., can solve problems such as difficult nanometer-sized composite nanocapsule materials, and achieve large specific surface area and high coating efficiency , the effect of reducing the damage of the capsule structure
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[0052] The preparation method of the composite nanocapsule phase change material mentioned above refers to the synergy between the interfacial polymerization reaction and the hydrolysis reaction, which well controls the overall reaction speed of the reaction system, so that the prepared composite nanocapsule phase change material has a good The uniformity and stability of the structure are used to control the primary particle size of the composite nanocapsule phase change material to be 50-400 nanometers and the average particle size to be 50-400 nanometers.
[0053] The introduction of ammonium persulfate, which can be used as both a monomer initiator and an ester hydrolysis catalyst, enables the interfacial polymerization reaction of methyl methacrylate and the interfacial hydrolysis reaction of ethyl orthosilicate to proceed simultaneously, which further improves the phase of the composite nanocapsules. The uniformity and stability of the structure of the variable material can ...
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[0056] Example 1
[0057] Preparation of composite nanocapsule phase change material
[0058] (1) A mixture of paraffin, methyl methacrylate and ethyl orthosilicate in the oil phase at a mass ratio of 6:9:1 is obtained;
[0059] (2) After dispersing the above mixture uniformly by ultrasound for 2 minutes, add it to a 500mL round bottom flask, stir with sheet-shaped stainless steel, heat it to 60℃ in a water bath at a stirring speed of 1500 rpm, and add 1 g of dodecane Sodium benzene sulfonate was added to 42.5 mL of deionized water to disperse uniformly, and added to a round bottom flask for emulsification for 20 minutes, then the temperature was raised to 80°C, and the emulsification was continued for 10 minutes at a stirring speed of 1500 rpm to obtain Uniform milky white microemulsion, in which the ratio of the mass of sodium dodecylbenzene sulfonate to the sum of the masses of paraffin, methyl methacrylate and ethyl orthosilicate in the oil phase is 1:13;
[0060] (3) After the e...
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[0065] Example 2
[0066] Preparation of composite nanocapsule phase change material
[0067] (1) Mix the oil phase paraffin, methyl methacrylate and ethyl orthosilicate in a mass ratio of 10:15:4 to obtain a mixture;
[0068] (2) After dispersing the above mixture uniformly by ultrasound for 2 minutes, add it to a 500mL round bottom flask, stir with sheet-shaped stainless steel, heat it to 60℃ in a water bath at a stirring speed of 1500 rpm, and add 1 g of dodecane Sodium benzene sulfonate was added to 42.5 mL of deionized water to disperse uniformly, and added to a round bottom flask for emulsification for 10 minutes, then the temperature was raised to 80°C, and the emulsification was continued for 20 minutes at a stirring speed of 1500 rpm to obtain Uniform milky white microemulsion, in which the ratio of the mass of sodium dodecylbenzene sulfonate to the sum of the masses of paraffin, methyl methacrylate and ethyl orthosilicate in the oil phase is 1:25;
[0069] (3) After the emu...
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