Preparation method of polyimide/graphene x-ray window film
A technology of polyimide and window film, which is applied in the field of preparation of X-ray window film, can solve the problems of difficult processing, poisonous beryllium window, use, etc., and achieve the effect of simple processing method, good processing formability and improved mechanical properties
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specific Embodiment approach 1
[0012] Embodiment 1: This embodiment is polyimide / graphene X-ray window film, which is prepared from graphene or graphene oxide, diamine monomer, dianhydride monomer and organic solvent. The graphene The mass ratio of the diamine monomer to the diamine monomer is 0.01:1, or the mass ratio of the graphene oxide to the diamine monomer is 0.01:1; the molar ratio of the dianhydride monomer to the diamine monomer is 1 : 1; the mass ratio of the volume of the organic solvent to the diamine monomer is 13.3mL: 1g.
[0013] As a special engineering material, polyimide film is widely used in aviation, aerospace, microelectronics, nanometer, liquid crystal, separation membrane, laser and other fields. Because of its outstanding features in performance and synthesis, its huge application prospects, whether as structural materials or functional materials, have been fully recognized. Thermosetting polyimide has excellent thermal and mechanical properties. The initial thermal decomposition ...
specific Embodiment approach 2
[0017] Embodiment 2: The difference between this embodiment and Embodiment 1 is that the diamine monomer is diaminodiphenyl ether, p-phenylenediamine, 4,4'-diaminodiphenyl sulfone or 4, 4 Diaminodiphenylmethane. Others are the same as the first embodiment.
specific Embodiment approach 3
[0018] Embodiment 3: The difference between this embodiment and Embodiment 1 or 2 is that the organic solvent is N'N-dimethylacetamide, N'N-dimethylformamide or N-formaldehyde base pyrrolidone. Others are the same as those in Embodiment 1 or 2.
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