Frame sealing adhesive for multi-dimensional electric field mode liquid crystal display panel and manufacture method of frame sealing adhesive
A multi-dimensional electric field and liquid crystal panel technology, which is applied in optics, instruments, nonlinear optics, etc., can solve the problems of high production cost of liquid crystal display and complex design of APR plate, etc., to simplify design and production, optimize coating process, and save production cost effect
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Embodiment 1
[0072] Example 1: Preparation of frame sealant 1
[0073] Put the epoxy resin shown in 100g formula (2) and 0.05g polymerization inhibitor p-hydroxyanisole into 500ml four-necked flask, wherein four are respectively connected with stirrer, condenser tube, thermometer and dropping funnel, put 53g The acrylic acid represented by formula (3) and 1.5 g of catalyst tetraethylammonium bromide were put into the dropping funnel, and the four-necked flask and the dropping funnel were fixed on the iron stand, and the preheating temperature was 70°C. Stir the solution in the four-necked flask, slowly drop the mixed solution of tetraethylammonium bromide and acrylic acid at a rate of 1 drop / second, after the dropwise addition, raise the temperature to 100°C, react for 8 hours, and cool to obtain the sealing frame of the present invention Glue 1.
Embodiment 2
[0074] Example 2: Preparation of frame sealant 2
[0075] Put the epoxy resin shown in 100g formula (2) and 0.05g polymerization inhibitor p-hydroxyanisole into 500ml four-necked flask, wherein four are respectively connected with stirrer, condenser tube, thermometer and dropping funnel, put 53g The acrylic acid represented by formula (3) and 1.5 g of catalyst tetraethylammonium bromide were put into the dropping funnel, and the four-necked flask and the dropping funnel were fixed on the iron stand, and the preheating temperature was 70°C. Stir the solution in the four-necked flask, slowly drop the mixed solution of tetraethylammonium bromide and acrylic acid at a rate of 1 drop / second, after the dropwise addition, raise the temperature to 100°C, react for 8 hours, and cool to obtain the sealing frame of the present invention glue2.
Embodiment 3
[0076] Embodiment 3: Preparation of frame sealant 3
[0077] Put the epoxy resin shown in 100g formula (2) and 0.05g polymerization inhibitor p-hydroxyanisole into 500ml four-necked flask, wherein four are respectively connected with stirrer, condenser tube, thermometer and dropping funnel, put 53g The acrylic acid represented by formula (3) and 1.5 g of catalyst tetraethylammonium bromide were put into the dropping funnel, and the four-necked flask and the dropping funnel were fixed on the iron stand, and the preheating temperature was 70°C. Stir the solution in the four-necked flask, slowly drop the mixed solution of tetraethylammonium bromide and acrylic acid at a rate of 1 drop / second, after the dropwise addition, raise the temperature to 100°C, react for 8 hours, and cool to obtain the sealing frame of the present invention glue3.
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