Method for preparing nano carbon electrode
A nanocarbon and electrode technology, applied in battery electrodes, nanotechnology, nanotechnology, etc., can solve the problems of increasing the amount of raw materials by agglomeration of carbon nanotubes, difficult to fully disperse carbon nanotubes, and reducing the capacity of composite materials. Effective reaction area, conducive to electrolyte storage, and the effect of improving high-rate performance
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Embodiment 1
[0033] 1) The liquid high molecular weight hydrocarbon precursor C with a volume ratio of 1:1:1 20 h 40 、C 20 h 42 and C 22 h44 Vaporization at 500°C to form a precursor gas;
[0034] 2) Weigh raw materials according to the following components and mass percentage content: catalyst 5g, lithium salt 5g, iron salt 50g and phosphate 30g; Described catalyst is the superfine powder of metal Ni, Y, Zr and MgO, and size is 500nm, its percentage by weight is respectively 85%, 5%, 5% and 10% of the total weight of the catalyst; the lithium salt is a combination of lithium carbonate, lithium hydroxide, lithium nitrate and lithium phosphate, and its percentage by weight is respectively lithium 45%, 25%, 25% and 5% of the total weight of the salt; the iron salt is ferrous oxalate and ferric phosphate, and its weight percentage is respectively 70% and 30% of the total weight of the iron salt; the phosphate It is ammonium dihydrogen phosphate and ammonium phosphate, and its weight perc...
Embodiment 2
[0042] 1) The liquid high molecular weight hydrocarbon precursor C with a volume ratio of 1:1:1 20 h 40 、C 20 h 42 and C 22 h 44 Vaporization at 500°C to form a precursor gas;
[0043] 2) Weigh raw materials according to the following components and mass percentage content: catalyst 5g, lithium salt 10g, iron salt 55g and phosphate 40g; Described catalyst is the superfine powder of metal Ni, Y, Zr and MgO, and size is 500nm, its percentage by weight is respectively 85%, 5%, 5% and 10% of the total weight of the catalyst; the lithium salt is a combination of lithium carbonate, lithium hydroxide, lithium nitrate and lithium phosphate, and its percentage by weight is respectively lithium 45%, 25%, 25% and 5% of the total weight of the salt; the iron salt is ferrous oxalate and ferric phosphate, and its weight percentage is respectively 70% and 30% of the total weight of the iron salt; the phosphate It is ammonium dihydrogen phosphate and ammonium phosphate, and its weight p...
Embodiment 3
[0051] 1) The liquid high molecular weight hydrocarbon precursor C with a volume ratio of 1:1:1 20 h 40 、C 20 h 42 and C 22 h 44 Vaporization at 500°C to form a precursor gas;
[0052] 2) Weigh raw materials according to the following components and mass percentage content: catalyst 10g, lithium salt 5g, iron salt 50g and phosphate 35g; Described catalyst is the superfine powder of metal Ni, Y, Zr and MgO, and size is 500nm, its percentage by weight is respectively 85%, 5%, 5% and 10% of the total weight of the catalyst; the lithium salt is a combination of lithium carbonate, lithium hydroxide, lithium nitrate and lithium phosphate, and its percentage by weight is respectively lithium 45%, 25%, 25% and 5% of the total weight of the salt; the iron salt is ferrous oxalate and ferric phosphate, and its weight percentage is respectively 70% and 30% of the total weight of the iron salt; the phosphate It is ammonium dihydrogen phosphate and ammonium phosphate, and its weight p...
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