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Blumea oil composite microcapsule, preparation method thereof and multifunctional textile preparation method

A technology of composite microcapsules and mugwort leaf oil, which is applied in the direction of microcapsule preparation, microsphere preparation, textiles and papermaking, etc., can solve the problems of complex preparation process, poor finishing reaction effect of microcapsule textiles, and low utilization rate of microcapsules, etc. To achieve the effect of enriching sources, prolonging the time of drug effect, and promoting wound healing

Inactive Publication Date: 2014-06-18
THE HONG KONG POLYTECHNIC UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0007] The technical problem to be solved by the present invention is to provide a kind of composite microcapsule of Artemisia argyi oil for the defects of cytotoxic substances in the artemisia leaf oil microcapsule; another technical problem to be solved by the present invention is to In order to solve the defects of complex preparation process and low utilization rate of the prepared microcapsules, a method for preparing mugwort leaf oil composite microcapsules is provided; another technical problem to be solved by the present invention is to finish the microcapsule textiles prepared in the prior art The defect of poor reaction effect provides a preparation method of multifunctional textiles containing mugwort leaf oil composite microcapsules

Method used

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  • Blumea oil composite microcapsule, preparation method thereof and multifunctional textile preparation method
  • Blumea oil composite microcapsule, preparation method thereof and multifunctional textile preparation method
  • Blumea oil composite microcapsule, preparation method thereof and multifunctional textile preparation method

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Effect test

Embodiment 1

[0043] 1. Preparation of mugwort leaf oil composite microcapsules

[0044] 1. Under the action of magnetic stirring, dissolve sodium alginate in water at 80°C to prepare a sodium alginate solution with a mass volume concentration of 0.5%, that is, 1 liter of water contains 5 mg of sodium alginate;

[0045] 2. Dissolve gelatin in water at 45°C to prepare a gelatin solution with a mass volume concentration of 4%, that is, 1 liter of water contains 40 mg of gelatin;

[0046] 3. Take 100mL each of the sodium alginate solution obtained in step 1 and the gelatin solution obtained in step 2 and mix them evenly, then add 0.5g of emulsifier Tween-80 and 1g of mugwort leaf oil to the mixed solution, and stir them evenly at 1500r / min The rotational speed high-speed shearing emulsification 5min, obtains mugwort leaf oil composite microcapsule emulsion, see for example figure 1 ;

[0047] 4. Keep the mugwort leaf oil composite microcapsule emulsion obtained in step 3 at 50°C, use a spray...

Embodiment 2

[0083] 1. Preparation of mugwort leaf oil composite microcapsules

[0084] 1. Under the action of magnetic stirring, dissolve sodium alginate in water at 80°C to prepare a sodium alginate solution with a mass volume concentration of 1%, that is, 1 liter of water contains 10 mg of sodium alginate;

[0085]2. Dissolve gelatin in water at 45°C to prepare a gelatin solution with a mass volume concentration of 6%, that is, 1 liter of water contains 60 mg of gelatin;

[0086] 3. Take 100mL each of the sodium alginate solution obtained in step 1 and the gelatin solution obtained in step 2 and mix well, add 1g of emulsifier Tween-80 and 2g of mugwort leaf oil to the mixed solution, stir well and then use 3000r / min Rotating speed and high-speed shear emulsification for 5 minutes to obtain the compound microcapsule emulsion of Artemisia argyi leaf oil.

[0087] 4. Keep the mugwort leaf oil composite microcapsule emulsion obtained in step 3 at 60°C, use a spray dryer to spray at an inle...

Embodiment 3

[0108] 1. Preparation of mugwort leaf oil composite microcapsules

[0109] 1. Under the action of magnetic stirring, dissolve sodium alginate in water at 80°C to prepare a sodium alginate solution with a mass volume concentration of 2%, that is, 1 liter of water contains 20 mg of sodium alginate;

[0110] 2. Dissolve gelatin in water at 45°C to prepare a gelatin solution with a mass volume concentration of 8%, that is, 1 liter of water contains 80 mg of gelatin;

[0111] 3. Take 100mL each of the sodium alginate solution obtained in step 1 and the gelatin solution obtained in step 2 and mix well, add 1g of emulsifier Tween-80 and 3g of mugwort leaf oil to the mixed solution, stir well and then use 3000r / min Rotating speed and high-speed shear emulsification for 10 minutes to obtain the mugwort leaf oil composite microcapsule emulsion.

[0112] 4. Keep the mugwort leaf oil composite microcapsule emulsion obtained in step 3 at 60°C, and use a spray dryer to spray at an inlet te...

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Abstract

The invention relates to a blumea oil microcapsule including a capsule core material and a capsule wall material with the mass ratio of 1:4 to 1:2, and the capsule wall material includes sodium alginate and gelatin with the mass ratio of 1:2 to 1:8. The invention also provides a preparation method of the microcapsule, and the preparation method using a spray drying method is simple and practicable, mild in condition, and easy in production; the microcapsule is prepared by using water as a solvent to avoid environmental pollution caused by the use of organic solvents. The invention also provides a multifunctional textile preparation method using 2D resin as an anti-wrinkle crosslinking agent, on the one hand through chemical bond 2D resin, a bridge grafting effect is played, and the composite microcapsule is grafted to a textile to prepare a multifunctional textile; on the other hand, capsule wall is cross linked and cured by use of free formaldehyde released by the 2D resin, the formaldehyde release amount of the finished textile is reduced, the sealing performance of the microcapsule wall is increased, the action time is prolonged, the microcapsule on the finished textile is insoluble in water, and the textile water-washing resistance is improved.

Description

technical field [0001] The present invention relates to the field of medicine microcapsule preparation technology and textile functional treatment, more specifically, relates to a kind of mugwort leaf oil composite microcapsule prepared by spray drying method and its specific preparation method, and multifunctional mugwort leaf oil composite microcapsule Preparation methods and applications of textiles. Background technique [0002] Microcapsule technology is a protective technology that encapsulates reactive, volatile, sensitive or odorous substances (core materials) through film-forming materials (wall materials) to form tiny particles. The process is called microencapsulation, and the tiny particles formed are called microcapsules. Microcapsule technology can achieve the purpose of controlling the release of core materials, protecting sensitive components, reducing or masking bad taste, isolating components, and turning liquid substances into pseudo-solids. With the con...

Claims

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Application Information

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IPC IPC(8): B01J13/04D06M23/12D06M11/76
Inventor 李鹂汪国成区伟文钟慧仪
Owner THE HONG KONG POLYTECHNIC UNIV
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