Calcium phosphate biofilm layer and its pulse electrochemical modification method
A biofilm layer, electrochemical technology, applied in electrolytic inorganic material coating and other directions, can solve the problems of low binding force between calcium and phosphorus salt film layer and metal substrate, difficult to achieve industrial application, etc., to improve comprehensive biological performance, morphology and size Controllable and stable effects
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[0028] (1) Example of changing Vn:
[0029] In the electrochemical modification method of this embodiment, the effect of Vn on the microstructure of OCP is mainly observed by changing the value of Vn, which specifically includes the following steps: pretreating the implant and putting the implant into a dilute acid solution Vibrate in the medium for 90 seconds, ultrasonically clean in deionized water for 30 seconds, take it out and dry for later use; prepare the electrolyte, the electrolyte concentration is 0.042mol / LCa(NO 3 ) 2 With a concentration of 0.028mol / LNH 4 H 2 PO 4 The pH value of the electrolyte is 4.2; electrochemical deposition is carried out in the electrolyte at a heating temperature of 80℃, the pretreated implant is used as the cathode, and the platinum electrode is used as the anode. Deposition. Among them, V'is -1.1V, T'is 20 seconds; Vn is -2.7V, -2.5V, -2.0V, -1.5V respectively, keep Tn for 15 seconds; potential V1 is -2.4V, keep T1 as 30 seconds; potential ...
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