Method for preparing fine-grained magnesium alloy with superplastic deformability

A magnesium alloy and superplastic technology, which is applied in the field of rolling and preparation of fine-grained magnesium alloys with superplastic deformation ability, and can solve the problems of difficulty in obtaining superplastic deformation characteristics, disadvantage of sheet strength stamping and forming, and difficulty in preparing large-sized materials. , to achieve the effect of easy operation, improve forming ability and reduce cracking

Active Publication Date: 2014-06-25
JILIN UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

For the traditional rolling method, due to its completely symmetrical upper and lower roll speeds, roll diameters and surface conditions, a strong basal texture will be produced in the rolled plate, resulting in a large grain size in the material structure, and it is difficult to obtain super Plastic deformation characteristics are very unfavorable to the strength of the plate and subsequent stamping forming, thus limiting its application
At present, the existing methods for preparing fine-grained superplastic magnesium alloys mainly include stack rolling method, spinning method, friction stir modification method, and equal channel extrusion method, etc., which are mainly used to prepare small samples for experiments, and it is difficult to prepare large-sized magnesium alloys. materials, and it is difficult to achieve large-scale mass production

Method used

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  • Method for preparing fine-grained magnesium alloy with superplastic deformability
  • Method for preparing fine-grained magnesium alloy with superplastic deformability

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0021] (1) Put the commercial AZ91 magnesium alloy billet into a heating box for heating. After the temperature rises to 380 degrees Celsius, let it stand for 100 minutes and then push the magnesium alloy billet horizontally to the roll entrance for two passes and a single pass. The vectors are horizontal rolling with small reductions of 8% and 6% respectively;

[0022] (2) Put the sample rolled in the above step (1) into the heating box again, let it stand for 30 minutes and keep it warm for one pass. The upper and lower rolls have an allometric ratio of 1.3 and a single pass reduction of 35%. Reduction in longitudinal asynchronous rolling;

[0023] (3) Put the sample after rolling in the above step (2) into the heating box again, let it stand for 20 minutes, and then carry out 8 passes of rolling, and after each rolling, perform a 180-degree longitudinal direction change;

[0024] (4) Reduce the temperature of the heating box to 210 degrees Celsius, put the sample rolled in the ab...

Embodiment 2

[0027] (1) Put the commercial AZ91 magnesium alloy extruded billet into a heating box for heating. After the temperature is raised to 350 degrees Celsius, let it stand for 80 minutes and then push the magnesium alloy billet horizontally to the roll entrance for 2 passes and single pass Lateral rolling with small reductions of 7% and 6% respectively;

[0028] (2) Put the sample rolled in the above step (1) into the heating box again, let it stand for 50 minutes and keep it warm for one pass. The upper and lower rolls have a different speed ratio of 1.4 and a single pass reduction of 38%. Reduction in longitudinal asynchronous rolling;

[0029] (3) Put the sample after rolling in the above step (2) into the heating box again, leave it to stand for 15 minutes, and then perform 10 passes of rolling, and after each rolling, perform a 180-degree longitudinal direction change;

[0030] (4) Lower the temperature of the heating box to 170 degrees Celsius, put the sample rolled in the above s...

Embodiment 3

[0033] (1) Put the commercial AZ61 magnesium alloy billet into a heating box for heating. After the temperature is raised to 320 degrees Celsius, let it stand for 145 minutes and then push the magnesium alloy billet horizontally to the roll entrance for 3 passes and a single pass. Horizontal rolling with small reductions of 6%, 7%, and 6% respectively;

[0034] (2) Put the sample rolled in the above step (1) into the heating box again, let it stand for 17 minutes, and perform one pass, the upper and lower rolls have an allometric ratio of 1.1, and a single pass reduction of 29%. Reduction in longitudinal asynchronous rolling;

[0035] (3) Put the sample after rolling in the above step (2) into the heating box again, let it stand for 30 minutes and keep it warm for 30 minutes, then perform 7 passes of rolling, and after each rolling, perform a 180-degree longitudinal direction change;

[0036] (4) Lower the temperature of the heating box to 290 degrees Celsius, put the sample rolled ...

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Abstract

The invention relates to a method for rolling fine-grained magnesium alloy with superplastic deformability. The method comprises the steps of low-rolling-reduction transverse rolling, high-rolling-reduction longitudinal asynchronous rolling, longitudinal reversed-direction rolling, low-temperature longitudinal rolling and annealing, and comprises the specific steps of heating a commercial magnesium alloy blank in a heating box, standing to preserve heat for a period of time after heating to a preset temperature, firstly pushing the magnesium alloy blank to an entrance of a rolling roller along the transverse direction, carrying out transverse rolling firstly, then, carrying out high-rolling-reduction longitudinal asynchronous rolling, then, carrying out longitudinal 180-degree-reversed rolling, then, carrying out low-temperature longitudinal rolling, and finally, carrying out low-temperature long-time annealing treatment or high-temperature short-time annealing treatment. According to the method, cracking during the rolling of the magnesium alloy can be reduced, the crystal grain of the magnesium alloy is refined, the texture is weakened, and the high-temperature plasticity of the magnesium alloy is improved; moreover, the process is simple and easy to operate, large-sized wide-width sheet materials can be prepared, and the formability of the magnesium alloy is improved remarkably, so that the method is applicable to the mass production of superplastic magnesium alloy and is prone to popularization and application.

Description

Technical field [0001] The invention relates to the field of metal materials, in particular to a rolling preparation method of a fine-grained magnesium alloy with superplastic deformation capability. Background technique [0002] Magnesium alloy is the lightest metal structural material in engineering applications. It has light specific gravity, high specific strength and specific rigidity, good damping, thermal conductivity, machinability, casting performance, strong electromagnetic shielding ability, stable size, rich resources, and easy Many advantages such as recycling have been increasingly used in the automotive industry, communications electronics, and aerospace industries. In recent years, the global annual growth rate of magnesium alloy production is as high as 20%, but compared with aluminum containing gold, the forming technology of magnesium alloy needs further development. Rolling is one of the most important processing and forming methods for magnesium alloy sheets...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C22F1/06
Inventor 王慧远张恩波于宏辰姜启川王金国王珵刘国军
Owner JILIN UNIV
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