Mesa etching process of high voltage diode silicon blocks

A high-voltage diode, mesa corrosion technology, applied in electrical components, semiconductor/solid-state device manufacturing, circuits, etc., can solve the problems of uneven silicon block mesa, uneven corrosion rate, junction tilt, etc., to improve yield and corrosion. The effect of small quantity difference and small reverse leakage

Active Publication Date: 2014-07-23
江苏皋鑫电子有限公司
View PDF3 Cites 5 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The traditional silicon block treatment process is a mixed acid etching composed of four components: nitric acid, hydrofluoric acid, sulfuric acid, and glacial acetic acid. During the silicon block etching process, the corrosion rate of the P surface and the N surface is unbalanced. After the treatment, the surface of the silicon block is uneven. Easy to produce gaps and inclined junctions

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024] 1) Mixed acid preparation: According to the ratio of nitric acid HNO3 (analytical pure AR, 65%): hydrofluoric acid HF (analytical pure AR, 40%): phosphoric acid H3PO4 (analytical pure AR, 85%)=5:3:5, To prepare 25 liters of mixed acid, add 1025 g of oxalic acid. Turn on the stirrer and stir until the oxalic acid is completely dissolved. Turn on the power of the cooling device and set the liquid temperature to 6°C;

[0025] 2) Put the silicon block to be processed into the BE plastic mold, and then install the BE mold with the silicon block on the plastic bracket;

[0026] 3) Mixed acid treatment: Turn on the main power supply of the acid etching device. Hang the bracket with the silicon block mold on the swing arm of the manipulator, set the mixed acid corrosion time to 150s, and set the swing arm frequency of the manipulator to 65 times / min. Turn on the switch of the manipulator, and the silicon block mold swings up and down for acid mixing treatment. During the tre...

Embodiment 2

[0039] 1) Mixed acid preparation: According to the ratio of nitric acid HNO3 (analytical pure AR, 67%): hydrofluoric acid HF (analytical pure AR, 40%): phosphoric acid H3PO4 (analytical pure AR, 85%)=5:3:5, To prepare 25 liters of mixed acid, add 1025 g of oxalic acid. Turn on the stirrer and stir until the oxalic acid is completely dissolved. Turn on the power of the cooling device and set the liquid temperature to 5°C;

[0040] 2) Put the silicon block to be processed into the BE plastic mold, and then install the BE mold with the silicon block on the plastic bracket;

[0041]3) Mixed acid treatment: Turn on the main power supply of the acid etching device. Hang the bracket with the silicon block mold on the swing arm of the manipulator, set the acid mix corrosion time to 140s, and set the swing arm frequency of the manipulator to 60 times / min. Turn on the switch of the manipulator, and the silicon block mold swings up and down for acid mixing treatment. During the treatm...

Embodiment 3

[0054] 1) Mixed acid preparation: According to the ratio of nitric acid HNO3 (analytical pure AR, 68%): hydrofluoric acid HF (analytical pure AR, 40%): phosphoric acid H3PO4 (analytical pure AR, 85%)=5:3:5, To prepare 25 liters of mixed acid, add 1025 g of oxalic acid. Turn on the stirrer and stir until the oxalic acid is completely dissolved. Turn on the power of the cooling device and set the liquid temperature to 7°C;

[0055] 2) Put the silicon block to be processed into the BE plastic mold, and then install the BE mold with the silicon block on the plastic bracket;

[0056] 3) Mixed acid treatment: Turn on the main power supply of the acid etching device. Hang the bracket with the silicon block mold on the swing arm of the manipulator, set the mixed acid corrosion time to 160s, and set the swing arm frequency of the manipulator to 70 times / min. Turn on the switch of the manipulator, and the silicon block mold swings up and down for acid mixing treatment. During the tre...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

No PUM Login to view more

Abstract

The invention relates to a mesa etching process of high voltage diode silicon blocks. The mesa etching process sequentially comprises performing mixed acid preparation; placing the silicon blocks to be treated into a BE plastic film and arranging the BE film with the silicon blocks on a plastic supporting frame; performing mixed acid treatment; performing etching quantity measurement; performing first time washing; performing nitric acid etching cleaning; performing second time washing; performing third time washing; performing dewatering and drying; drying the dry air; performing assembly sintering on the silicon blocks and electrode leads. According to the mesa etching process of the high voltage diode silicon blocks, a novel mixed acid is developed and accordingly the etching speed of cutting surfaces of the silicon blocks is consistent, the difference of the etching quantity is small, and damage layers caused by cut-off are completely removed; hydrofluoric acid cleaning treatment is performed after the mixed acid treatment is performed and accordingly a few oxidation layers on the surface of chip solder are removed and the good sintering soldering of the electrode leads can be convenient; the etching treatment rate is uniform and accordingly the good mesa shapes of the silicon blocks are formed and the difference of the etching quantity is small; the reverse electric leakage of a device is small, the breakdown characteristic is hard, the surge tolerance is large, and the rate of finished products is significantly improved.

Description

technical field [0001] The invention relates to a high-voltage diode silicon block mesa corrosion process, in particular to a process method for high-voltage diode chip mesa corrosion cleaning and mesa formation. Background technique [0002] The silicon stack is cut into a silicon block by stainless steel wire supplemented with emery cutting fluid, that is, a high-voltage diode die. The surface of the silicon block has damaged layers, oxide layers, and other impurities caused by cutting. Before the silicon block and electrode leads are sintered, the mesa must be cleaned. The electrical properties of the device. Otherwise, the electrical performance of the device will be deteriorated, and the yield of the electrical test of the product will be greatly reduced. [0003] The traditional silicon block treatment process is a mixed acid etching composed of four components: nitric acid, hydrofluoric acid, sulfuric acid, and glacial acetic acid. During the silicon block etching p...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
Patent Type & Authority Applications(China)
IPC IPC(8): H01L21/329H01L21/306
CPCH01L21/30604H01L29/6609
Inventor 陈许平
Owner 江苏皋鑫电子有限公司
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products